2,4-Dicumylphenol

Base Information

• Chemical Name: 2,4-Dicumylphenol
• CAS No.: 106060-52-0
• Molecular Formula: C₂₄H₂₆O
• Molecular Weight: 330.47
• Mol file: 106060-52-0.mol

Synonyms:

Chemical Property of 2,4-Dicumylphenol

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-Dicumylphenol

There total 10 articles about 2,4-Dicumylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.6%

p-cumylphenol (599-64-4) + isopropenylbenzene (98-83-9,6144-04-3,25014-31-7,42612-14-6) → 2,4-di-cumylphenol (2772-45-4,106060-52-0)

Guidance literature:

With toluene-4-sulfonic acid; In Petroleum ether; at 75 ℃; Inert atmosphere;

Reference yield: 94.6%

→ 2,4-di-cumylphenol (2772-45-4,106060-52-0)

Guidance literature:

With toluene-4-sulfonic acid; In Petroleum ether; at 75 ℃; Inert atmosphere;

Reference yield: 86.0%

isopropenylbenzene (98-83-9,6144-04-3,25014-31-7,42612-14-6) + phenol (108-95-2,27073-41-2) → p-cumylphenol (599-64-4) + 2,4-di-cumylphenol (2772-45-4,106060-52-0)

Guidance literature:

With decacarbonyldirhenium⁽⁰⁾; In toluene; at 150 ℃; for 24h; regioselective reaction; Inert atmosphere; Sealed tube;

DOI:10.1021/ja904360k

upstream raw materials:

isopropenylbenzene

phenol

p-cumylphenol

Refernces

• 1、 -. "Amino-acid schiff base, and synthesis method and application thereof". Paragraph 0078; 0079; 0120. . Retrieved 2017/09/18.
• 2、 -. "Ortho-aminophenol Schiff base, and synthesis method and application thereof". Paragraph 0071; 0073; 0074. . Retrieved 2017/12/05.