METHYL 5-BROMO-2-METHOXY-4-METHYLBENZOATE

Base Information

• Chemical Name: METHYL 5-BROMO-2-METHOXY-4-METHYLBENZOATE
• CAS No.: 39503-58-7
• Molecular Formula: C10H11BrO3
• Molecular Weight: 259.1
• Hs Code.: 2918990090
• Mol file: 39503-58-7.mol

Synonyms:METHYL 5-BROMO-2-METHOXY-4-METHYLBENZOATE;5-BroMo-2-Methoxy-4-Methyl-benzoic acid Methyl ester

Chemical Property of METHYL 5-BROMO-2-METHOXY-4-METHYLBENZOATE

Chemical Property:

• Vapor Pressure: 0.000355mmHg at 25°C
• Melting Point: 45-46 °C
• Boiling Point: 318.7°C at 760 mmHg
• Flash Point: 146.6°C
• PSA: 35.53000
• Density: 1.409g/cm³
• LogP: 2.55270
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

Methyl5-bromo-2-methoxy-4-methylbenzoate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of METHYL 5-BROMO-2-METHOXY-4-METHYLBENZOATE

There total 10 articles about METHYL 5-BROMO-2-METHOXY-4-METHYLBENZOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methyl 4-methyl-2-methoxybenzoate (81245-24-1) → methyl 5-bromo-2-methoxy-4-methylbenzoate (39503-58-7)

Guidance literature:

With bromine; acetic acid; at 20 - 25 ℃; for 2h;

Reference yield: 82.0%

5-bromo-2-hydroxy-4-methylbenzoic acid (6623-35-4) + methyl iodide (74-88-4) → methyl 5-bromo-2-methoxy-4-methylbenzoate (39503-58-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 17h;

Reference yield: 17.0%

methyl 5-bromo-2-hydroxy-4-methylbenzoate (39503-57-6) + methyl iodide (74-88-4) → methyl 5-bromo-2-methoxy-4-methylbenzoate (39503-58-7)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 - 40 ℃; for 17h;

DOI:10.1016/j.ejmech.2017.12.041

upstream raw materials:

5-bromo-2-hydroxy-4-methylbenzoic acid

dimethyl sulfate

methyl 4-methyl-2-methoxybenzoate

4'-hydroxy-2'-methylacetophenone

Downstream raw materials:

5-bromo-2-methoxy-4-methyl-3-nitro-benzoic acid methyl ester

5-bromo-2-methoxy-4-methyl-aniline

5-bromo-2-methoxy-4-methylbenzamide

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