6-methoxy-1,1-dimethyl-3,4-dihydronaphthalen-2(1H)-one

Base Information

Chemical Name:6-methoxy-1,1-dimethyl-3,4-dihydronaphthalen-2(1H)-one
CAS No.:71886-83-4
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:
Mol file:71886-83-4.mol

Synonyms:6-methoxy-1,1-dimethyl-3,4-dihydronaphthalen-2(1H)-one;3,4-dihydro-6-methoxy-1,1-dimethylnaphthalen-2(1H)-one

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-methoxy-1,1-dimethyl-3,4-dihydronaphthalen-2(1H)-one

Chemical Property:

Boiling Point:108-113 °C(Press: 0.5-0.6 Torr)
PSA：26.30000
Density:1.046±0.06 g/cm3(Predicted)
LogP:2.48810

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-methoxy-1,1-dimethyl-3,4-dihydronaphthalen-2(1H)-one

There total 10 articles about 6-methoxy-1,1-dimethyl-3,4-dihydronaphthalen-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.5%

: 2472-22-2
6-methoxy-2-tetralone

: 74-88-4
methyl iodide

: 71886-83-4
6-methoxy-1,1-dimethyl-3,4-dihydronaphthalene-2(1H)-one

Guidance literature:: With sodium hydride; In benzene; 1.) 5-10 deg C, 70 min, 2.) room temperature, 15 h.;
DOI:10.1021/jo01290a005

Reference yield: 71.0%

: 5111-67-1
1-methyl-6-methoxy-2-tetralone

: 74-88-4
methyl iodide

: 71886-83-4
6-methoxy-1,1-dimethyl-3,4-dihydronaphthalene-2(1H)-one

Guidance literature:: 1-methyl-6-methoxy-2-tetralone; With potassium hydride; In tetrahydrofuran; at 0 - 23 ℃; for 1.75h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at 0 - 23 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2019.03.010

Reference yield:

: 581-43-1
2.6-dihydroxynaphthalene

: 71886-83-4
6-methoxy-1,1-dimethyl-3,4-dihydronaphthalene-2(1H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: (i) Na, MeOH, (ii) /BRN= 609209/, dioxane

2: Na, 3-methyl-butan-1-ol

3: aq. HCO₂H

4: dioxane; diethyl ether / (methylation)

With formic acid; i-Amyl alcohol; sodium; In 1,4-dioxane; diethyl ether;
DOI:10.1021/jm00334a026