4-Aminobenzoic (4-methoxybenzylidene)hydrazide

Base Information

• Chemical Name: 4-Aminobenzoic (4-methoxybenzylidene)hydrazide
• CAS No.: 97742-06-8
• Molecular Formula: C₁₅H₁₅N₃O₂
• Molecular Weight: 269.303
• European Community (EC) Number: 659-145-9
• NSC Number: 204293
• ChEMBL ID: CHEMBL539406

Synonyms:NSC204293;CHEMBL539406;AKOS002262199;NSC-204293;4-AMINOBENZOIC (4-METHOXYBENZYLIDENE)HYDRAZIDE

Chemical Property of 4-Aminobenzoic (4-methoxybenzylidene)hydrazide

Chemical Property:

• XLogP3: 1.9
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 269.116426730
• Heavy Atom Count: 20
• Complexity: 330

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)C=NNC(=O)C2=CC=C(C=C2)N
• Isomeric SMILES: COC1=CC=C(C=C1)/C=N/NC(=O)C2=CC=C(C=C2)N

Technology Process of 4-Aminobenzoic (4-methoxybenzylidene)hydrazide

There total 1 articles about 4-Aminobenzoic (4-methoxybenzylidene)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

4-methoxy-benzaldehyde (123-11-5) + 4-aminobenzohydrazide (5351-17-7) → 4-amino-benzoic acid-(4-methoxy-benzylidenehydrazide) (97742-06-8)

Guidance literature:

In ethanol;

Reference yield: 82.0%

4-amino-benzoic acid-(4-methoxy-benzylidenehydrazide) (97742-06-8) + phenyl isothiocyanate (103-72-0) → 1-{4-[1-(4-Methoxy-phenyl)-meth-(E)-ylidene-hydrazinocarbonyl]-phenyl}-3-phenyl-thiourea

Guidance literature:

In 1,4-dioxane;

Reference yield: 28.9%

3-pyridinecarbonyl chloride (10400-19-8) + C15H15N3O2 (97742-06-8) → nicotinic acid N-(4-amino-benzoyl)-N'-(4-methoxybenzylidene)-hydrazide (1261627-63-7)

Guidance literature:

In diethyl ether; at 20 ℃; for 24h;

DOI:10.1016/j.ejmech.2010.08.030

upstream raw materials:

4-methoxy-benzaldehyde

4-aminobenzohydrazide

Downstream raw materials:

4-(1H-Indol-3-ylazo)-benzoic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

nicotinic acid N-(4-amino-benzoyl)-N'-(4-methoxybenzylidene)-hydrazide

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