Benzenepropanal, 2-broMo-4,5-diMethoxy- (or 3-(2-BroMo-4,5-diMethoxyphenyl)propanal )

Base Information

Chemical Name:Benzenepropanal, 2-broMo-4,5-diMethoxy- (or 3-(2-BroMo-4,5-diMethoxyphenyl)propanal )
CAS No.:958883-36-8
Molecular Formula:C11H13BrO3
Molecular Weight:273.12
Hs Code.:
Mol file:958883-36-8.mol

Synonyms:Benzenepropanal, 2-broMo-4,5-diMethoxy- (or 3-(2-BroMo-4,5-diMethoxyphenyl)propanal )

Suppliers and Price of Benzenepropanal, 2-broMo-4,5-diMethoxy- (or 3-(2-BroMo-4,5-diMethoxyphenyl)propanal )

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-BROMO-4,5-DIMETHOXY-BENZENEPROPANAL 95.00%
5MG
$ 497.20

Total 0 raw suppliers

Chemical Property of Benzenepropanal, 2-broMo-4,5-diMethoxy- (or 3-(2-BroMo-4,5-diMethoxyphenyl)propanal )

Chemical Property:

PSA：35.53000
LogP:2.59780

Purity/Quality:: 2-BROMO-4,5-DIMETHOXY-BENZENEPROPANAL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenepropanal, 2-broMo-4,5-diMethoxy- (or 3-(2-BroMo-4,5-diMethoxyphenyl)propanal )

There total 4 articles about Benzenepropanal, 2-broMo-4,5-diMethoxy- (or 3-(2-BroMo-4,5-diMethoxyphenyl)propanal ) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 89978-46-1
4-bromo-5-iodoveratrole

: 107-18-6
allyl alcohol

: 958883-36-8
3-(2-bromo-4,5-dimethoxyphenyl)propanal

Guidance literature:: With N-benzyl-N,N,N-triethylammonium chloride; palladium diacetate; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 40 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol800330d

Reference yield: 65.0%

: 125593-63-7
3-(2-bromo-4,5-dimethoxyphenyl)propan-1-ol

: 958883-36-8
3-(2-bromo-4,5-dimethoxyphenyl)propanal

Guidance literature:: With dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; at 20 ℃; for 8h;
DOI:10.1021/ja0733235

Reference yield:

: 52679-49-9
3-(2'-bromo-4',5'-dimethoxyphenyl)propionic acid

: 958883-36-8
3-(2-bromo-4,5-dimethoxyphenyl)propanal

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfide borane complex / tetrahydrofuran / 10 h / 0 - 60 °C / Inert atmosphere

2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

With dimethylsulfide borane complex; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.orglett.2c00153