1-Piperidinecarboxylicacid,4-hydrazino-,ethylester(9CI)

Base Information Edit

Chemical Name:1-Piperidinecarboxylicacid,4-hydrazino-,ethylester(9CI)
CAS No.:693287-94-4
Molecular Formula:C8H17N3O2
Molecular Weight:0
Hs Code.:
Mol file:693287-94-4.mol

Synonyms:1-Piperidinecarboxylicacid,4-hydrazino-,ethylester(9CI);4-Hydrazino-piperidine-1-carboxylic acid ethyl ester

Suppliers and Price of 1-Piperidinecarboxylicacid,4-hydrazino-,ethylester(9CI)

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 1-Piperidinecarboxylicacid,4-hydrazino-,ethylester(9CI) Edit

Chemical Property:

PSA：67.59000
LogP:1.09970

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Piperidinecarboxylicacid,4-hydrazino-,ethylester(9CI)

There total 4 articles about 1-Piperidinecarboxylicacid,4-hydrazino-,ethylester(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 693287-93-3
ethyl 4-{[(tert-butoxy)carbonylamino]amino}piperidinecarboxylate

: 693287-94-4
ethyl 4-hydrazinopiperidinecarboxylate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃;
DOI:10.1021/jm030276s

Reference yield:

: 870-46-2
t-butoxycarbonylhydrazine

: 29976-53-2
N-ethoxycarbonyl-4-piperidone

: 693287-94-4
ethyl 4-hydrazinopiperidinecarboxylate

Guidance literature:: t-butoxycarbonylhydrazine; N-ethoxycarbonyl-4-piperidone; In ethanol; for 24h;

With hydrogen; platinum on carbon; In ethanol; at 20 ℃; under 760.051 Torr;

Reference yield:

: 29976-53-2
N-ethoxycarbonyl-4-piperidone

: 693287-94-4
ethyl 4-hydrazinopiperidinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / methanol / 20 °C

2: 100 percent / sodium cyanoborohydride; aq. acetic acid / 20 °C

3: 100 percent / trifluoroacetic acid / CH₂Cl₂ / 20 °C

With sodium cyanoborohydride; acetic acid; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1021/jm030276s