1-(4-bromo-2-hydroxyphenyl)-2-(2,5-dibromophenyl)ethan-1-one

Base Information

Chemical Name:1-(4-bromo-2-hydroxyphenyl)-2-(2,5-dibromophenyl)ethan-1-one
CAS No.:1403991-85-4
Molecular Formula:C14H9Br3O2
Molecular Weight:448.936
Hs Code.:
Mol file:1403991-85-4.mol

Synonyms:1-(4-bromo-2-hydroxyphenyl)-2-(2,5-dibromophenyl)ethan-1-one;1-(4-bromo-2-hydroxyphenyl)-2-(2,5-dibromophenyl)ethanone;Ethanone, 1-(4-bromo-2-hydroxyphenyl)-2-(2,5-dibromophenyl)-

Suppliers and Price of 1-(4-bromo-2-hydroxyphenyl)-2-(2,5-dibromophenyl)ethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 13 raw suppliers

Chemical Property of 1-(4-bromo-2-hydroxyphenyl)-2-(2,5-dibromophenyl)ethan-1-one

Chemical Property:

Boiling Point:497.2±45.0 °C(Predicted)
PKA:6.80±0.35(Predicted)
PSA：37.30000
Density:1.963±0.06 g/cm3(Predicted)
LogP:5.10510

Purity/Quality:: 99.9% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(4-bromo-2-hydroxyphenyl)-2-(2,5-dibromophenyl)ethan-1-one

There total 6 articles about 1-(4-bromo-2-hydroxyphenyl)-2-(2,5-dibromophenyl)ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1403991-82-1
3-bromophenyl 2-(2,5-dibromophenyl)acetate

: 1403991-85-4
1-(4-bromo-2-hydroxyphenyl)-2-(2,5-dibromophenyl)ethanone

Guidance literature:: With methanesulfonic acid; Methanesulfonic anhydride; at 80 ℃; for 24h; Reagent/catalyst; Temperature;
DOI:10.1134/S107036322105025X

Reference yield:

: 203314-28-7
2-(2,5-dibromophenyl)-acetic acid

: 1403991-85-4
1-(4-bromo-2-hydroxyphenyl)-2-(2,5-dibromophenyl)ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 1 h / 20 °C / Inert atmosphere

2: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 5 °C / Inert atmosphere

3: Methanesulfonic anhydride; methanesulfonic acid / 65 °C / Inert atmosphere

With 2,6-dimethylpyridine; oxalyl dichloride; methanesulfonic acid; Methanesulfonic anhydride; In dichloromethane; N,N-dimethyl-formamide; 3: |Fries Phenol Ester Rearrangement;
DOI:10.1021/ol500971c

Reference yield:

: 203314-51-6
(2,5-dibromo-phenyl)-acetyl chloride

: 1403991-85-4
1-(4-bromo-2-hydroxyphenyl)-2-(2,5-dibromophenyl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 5 °C / Inert atmosphere

2: Methanesulfonic anhydride; methanesulfonic acid / 65 °C / Inert atmosphere

With 2,6-dimethylpyridine; methanesulfonic acid; Methanesulfonic anhydride; In dichloromethane; 2: |Fries Phenol Ester Rearrangement;
DOI:10.1021/ol500971c