3-IODO-4-METHYL-5-NITROMETHYL BENZOATE

Base Information

Chemical Name:3-IODO-4-METHYL-5-NITROMETHYL BENZOATE
CAS No.:21323-99-9
Molecular Formula:C9H8INO4
Molecular Weight:321.071
Hs Code.:2916399090
Mol file:21323-99-9.mol

Synonyms:3-IODO-4-METHYL-5-NITROMETHYL BENZOATE;methyl 3-iodo-4-methyl-5-nitrobenzoate

Suppliers and Price of 3-IODO-4-METHYL-5-NITROMETHYL BENZOATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemcia Scientific
3-Iodo-4-methyl-5-nitro-benzoicacidmethylester 95%
0.5 G
$ 450.00

Chemcia Scientific
3-Iodo-4-methyl-5-nitro-benzoicacidmethylester 95%
2.5 G
$ 1325.00

American Custom Chemicals Corporation
3-IODO-4-METHYL-5-NITROMETHYL BENZOATE 95.00%
5MG
$ 497.99

Total 8 raw suppliers

Chemical Property of 3-IODO-4-METHYL-5-NITROMETHYL BENZOATE

Chemical Property:

PSA：72.12000
LogP:2.81760

Purity/Quality:

97% ^*data from raw suppliers

3-Iodo-4-methyl-5-nitro-benzoicacidmethylester 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-IODO-4-METHYL-5-NITROMETHYL BENZOATE

There total 3 articles about 3-IODO-4-METHYL-5-NITROMETHYL BENZOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 67-56-1
methanol

: 21312-29-8
3-iodo-4-methyl-5-nitro-benzoic acid

: 21323-99-9
methyl 3-iodo-4-methyl-5-nitrobenzoate

Guidance literature:: With potassium carbonate; In acetone; at 40 ℃;

Reference yield:

: 72922-60-2
methyl 3-amino-4-methyl-5-nitrobenzoate

: 21323-99-9
methyl 3-iodo-4-methyl-5-nitrobenzoate

Guidance literature:: methyl 3-amino-4-methyl-5-nitrobenzoate; With hydrogenchloride; sodium nitrite; In water; for 1.33h; Cooling with ice;

With potassium iodide; In water; at 20 ℃; for 2.33h; Cooling with ice;

Reference yield:

: 54591-62-7
3-amino-4-methyl-5-nitrobenzoic acid

: 21323-99-9
methyl 3-iodo-4-methyl-5-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: (i) aq. NaNO₂, HCl, (ii) KI

2: H₂SO₄

With sulfuric acid;
DOI:10.1021/jm00301a007