1-(Tert-butyl)-3,5-diiodo-2-methoxybenzene

Base Information

Chemical Name:1-(Tert-butyl)-3,5-diiodo-2-methoxybenzene
CAS No.:1132940-51-2
Molecular Formula:C₁₁H₁₄I₂O
Molecular Weight:416.041
Hs Code.:
DSSTox Substance ID:DTXSID901335211
Mol file:1132940-51-2.mol

Synonyms:1-(TERT-BUTYL)-3,5-DIIODO-2-METHOXYBENZENE;1132940-51-2;1-tert-butyl-3,5-diiodo-2-methoxybenzene;SCHEMBL351682;PBISNKVQOXSGFO-UHFFFAOYSA-N;DTXSID901335211;AM808010;FT-0733741;A907408;1,5-Diiodo-2-methoxy-3-(2-methyl-2-propanyl)benzene

Suppliers and Price of 1-(Tert-butyl)-3,5-diiodo-2-methoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of 1-(Tert-butyl)-3,5-diiodo-2-methoxybenzene

Chemical Property:

XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:415.91341
Heavy Atom Count:14
Complexity:188

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1=C(C(=CC(=C1)I)I)OC

Technology Process of 1-(Tert-butyl)-3,5-diiodo-2-methoxybenzene

There total 4 articles about 1-(Tert-butyl)-3,5-diiodo-2-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 74-88-4
methyl iodide

: 60803-26-1
2-(tert-butyl)-4,6-diiodophenol

: 1132940-51-2
1-tert-butyl-3,5-diiodo-2-methoxybenzene

Guidance literature:: With sodium hydroxide; In water; acetone; at 20 ℃; for 48h; Product distribution / selectivity;

Reference yield: 92.0%

: 88-18-6
2-tert-Butylphenol

: 74-88-4
methyl iodide

: 1132940-51-2
1-tert-butyl-3,5-diiodo-2-methoxybenzene

: C₁₁H₁₄ClIO

Guidance literature:: 2-tert-Butylphenol; With sodium hydroxide; In methanol; at 20 ℃;

With hydrogenchloride; sodium hypochlorite; sodium thiosulfate; sodium iodide; In methanol; water; at 0 ℃;

methyl iodide; With sodium hydroxide; In water; acetone;
DOI:10.1021/acs.joc.8b02690

Reference yield:

: 39068-23-0
sodium 2-tert-butylphenolate

: 1132940-51-2
1-tert-butyl-3,5-diiodo-2-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium iodide; sodium hypochlorite / methanol / 0 °C

1.2: 1.62 h / 1.2 - 4.1 °C / pH 3

2.1: sodium hydroxide / water; acetone

With sodium hypochlorite; sodium iodide; sodium hydroxide; In methanol; water; acetone;