2,2'-Bipyridine-4,4'-dicarboxamide

Base Information

• Chemical Name: 2,2'-Bipyridine-4,4'-dicarboxamide
• CAS No.: 100137-02-8
• Molecular Formula: C12H10N4O2
• Molecular Weight: 242.237
• Mol file: 100137-02-8.mol

Synonyms:2,2'-Bipyridine-4,4'-dicarboxamide;4,4'-Dicarbamoyl-2,2'-bipyridine

Chemical Property of 2,2'-Bipyridine-4,4'-dicarboxamide

Chemical Property:

• PSA: 111.96000
• LogP: 1.74200
• Storage Temp.: Refrigerator

Purity/Quality:

97% ^*data from raw suppliers

2,2''-Bipyridine-4,4''-dicarboxamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2'-Bipyridine-4,4'-dicarboxamide

There total 5 articles about 2,2'-Bipyridine-4,4'-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2'-Bipyridine-4,4'-dicarboxylic acid (6813-38-3) → 2,2'-bipyridine-4,4'-bis(carboxamide) (100137-02-8)

Guidance literature:

Multi-step reaction with 2 steps

2: ammonia

With ammonia;

DOI:10.1016/0022-328X(88)89021-1

Reference yield:

4,4'-dimethyl-2,2'-bipyridines (1134-35-6) → 2,2'-bipyridine-4,4'-bis(carboxamide) (100137-02-8)

Guidance literature:

Multi-step reaction with 3 steps

1: oxidation

3: ammonia

With ammonia;

DOI:10.1016/0022-328X(88)89021-1

Reference yield:

2,2'-bipyridyl-4,4'-dicarboxylic acid chloride (72460-28-7) → 2,2'-bipyridine-4,4'-bis(carboxamide) (100137-02-8)

Guidance literature:

With ammonia;

DOI:10.1016/0022-328X(88)89021-1

upstream raw materials:

2,2'-bipyridyl-4,4'-dicarboxylic acid chloride

4,4'-bis(ethoxycarbonyl)-2,2'-bipyridine

ammonia

picoline

Downstream raw materials:

2,2’-bipyridine-4,4’-dicarbonitrile

Refernces

• 1、 Turlington, Michael D.,Troian-Gautier, Ludovic,Sampaio, Renato N.,Beauvilliers, Evan E.,Meyer, Gerald J.. "Control of Excited-State Supramolecular Assembly Leading to Halide Photorelease". . p. 3316 - 3328. Retrieved 2019.