3,5-Dibromotricyclo[2.2.1.02,6]heptane

Base Information

Chemical Name:3,5-Dibromotricyclo[2.2.1.02,6]heptane
CAS No.:5473-09-6
Molecular Formula:
Molecular Weight:0
Hs Code.:
NSC Number:29646
DSSTox Substance ID:DTXSID00970052

Synonyms:5473-09-6;NSC29646;DTXSID00970052;NSC-29646;3,5-Dibromotricyclo[2.2.1.0~2,6~]heptane

Suppliers and Price of 3,5-Dibromotricyclo[2.2.1.02,6]heptane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3,5-Dibromotricyclo[2.2.1.02,6]heptane

Chemical Property:

Vapor Pressure:0.0355mmHg at 25°C
Boiling Point:249.8°C at 760 mmHg
Flash Point:115.4°C
Density:2.191g/cm³
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:251.89723
Heavy Atom Count:9
Complexity:152

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2C3C2C(C1C3Br)Br

Technology Process of 3,5-Dibromotricyclo[2.2.1.02,6]heptane

There total 21 articles about 3,5-Dibromotricyclo[2.2.1.02,6]heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 121-46-0
bicyclo[2.2.1]hepta-2,5-diene

: (2-exo,3-exo)-2-bromo-3-nitrosobicyclo[2.2.1]hept-5-ene

: 5473-09-6,75685-55-1,75685-56-2
exo,exo-3,5-dibromotricyclo<2.2.1.0^2,6>heptane

: 5473-09-6,75685-55-1,75685-56-2
exo,endo-3,5-dibromotricyclo<2.2.1.0^2,6>heptane

: 75649-50-2,75649-51-3,89694-72-4
(5-exo,7-syn)-5,7-dibromotricyclo[2.2.1.0^2,6]heptane

Guidance literature:: With ethyl nitrite; phosphorus tribromide; In chloroform; at -30 - 20 ℃;
DOI:10.1007/s11172-006-0088-3

Reference yield: 60.0%

: 121-46-0
bicyclo[2.2.1]hepta-2,5-diene

: (2-exo,3-exo)-2-bromo-3-nitrosobicyclo[2.2.1]hept-5-ene

: 5473-09-6,75685-55-1,75685-56-2
exo,exo-3,5-dibromotricyclo<2.2.1.0^2,6>heptane

: 5473-09-6,75685-55-1,75685-56-2
exo,endo-3,5-dibromotricyclo<2.2.1.0^2,6>heptane

: 75649-50-2,75649-51-3,89694-72-4
(5-exo,7-syn)-5,7-dibromotricyclo[2.2.1.0^2,6]heptane

Guidance literature:: With ethyl nitrite; phosphorus tribromide; In chloroform; at -30 - 20 ℃;
DOI:10.1007/s11172-006-0088-3

Reference yield: 7.0%

: 121-46-0
bicyclo[2.2.1]hepta-2,5-diene

: 5473-09-6,75685-55-1,75685-56-2
exo,exo-3,5-dibromonortricyclane

: 5473-09-6,75685-55-1,75685-56-2
3-exo-5-endo-dibrimonontricyclane

: (1R,2R,3S,4R,5R,6S)-2,3,5,6-Tetrabromo-bicyclo[2.2.1]heptane

: (1S,2S,3S,4R,5R,6S)-2,3,5,6-Tetrabromo-bicyclo[2.2.1]heptane

Guidance literature:: With bromine; In tetrachloromethane; at 77 ℃; for 0.0833333h; Further byproducts given; further reagent: 2,4,6-tri-tert-butylphenol;
DOI:10.1021/jo960225l