ethyl 2-aMino-5,6-diMethoxy-1H-indole-3-carboxylate

Base Information

Chemical Name:ethyl 2-aMino-5,6-diMethoxy-1H-indole-3-carboxylate
CAS No.:121641-88-1
Molecular Formula:C₁₃H₁₆N₂O₄
Molecular Weight:264.281
Hs Code.:
Mol file:121641-88-1.mol

Synonyms:ethyl 2-aMino-5,6-diMethoxy-1H-indole-3-carboxylate;2-amino-5,6-dimethoxy-1H-Indole-3-carboxylic acid ethyl ester

Suppliers and Price of ethyl 2-aMino-5,6-diMethoxy-1H-indole-3-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of ethyl 2-aMino-5,6-diMethoxy-1H-indole-3-carboxylate

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:451.379°C at 760 mmHg
Flash Point:226.786°C
Density:1.279g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ethyl 2-aMino-5,6-diMethoxy-1H-indole-3-carboxylate

There total 4 articles about ethyl 2-aMino-5,6-diMethoxy-1H-indole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 913837-98-6
ethyl 2-cyano-2-(4,5-dimethoxy-2-nitro-phenyl)-acetate

: 121641-88-1
5,6-dimethoxy-2-amino-3-carbethoxyindole

Guidance literature:: With acetic acid; zinc; at 65 ℃; for 12h;

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 121641-88-1
5,6-dimethoxy-2-amino-3-carbethoxyindole

Guidance literature:

Reference yield:

: 16766-27-1
4-chloro-1,2-dimethoxybenzene

: 121641-88-1
5,6-dimethoxy-2-amino-3-carbethoxyindole

Guidance literature:: Multi-step reaction with 3 steps

1.1: nitric acid / 1.5 h / 25 °C

2.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / 0 °C

2.2: 24 h / Heating / reflux

3.1: acetic acid; zinc / 12 h / 65 °C

With potassium tert-butylate; nitric acid; acetic acid; zinc; In tetrahydrofuran;