4-Bromo-2-iodophenyl trifluoromethyl ether, 4-Bromo-2-iodo-alpha,alpha,alpha-trifluoroanisole

Base Information

• Chemical Name: 4-Bromo-2-iodophenyl trifluoromethyl ether, 4-Bromo-2-iodo-alpha,alpha,alpha-trifluoroanisole
• CAS No.: 154065-33-5
• Molecular Formula: C7H3BrF3IO
• Molecular Weight: 366.904
• Hs Code.: 2909309090
• Mol file: 154065-33-5.mol

Synonyms:4-Bromo-2-iodo-1-(trifluoromethoxy)benzene;4-Bromo-2-iodophenyl trifluoromethyl ether, 4-Bromo-2-iodo-alpha,alpha,alpha-trifluoroanisole;4-BroMo-2-iodo(trifluoroMethoxy)benzene

Chemical Property of 4-Bromo-2-iodophenyl trifluoromethyl ether, 4-Bromo-2-iodo-alpha,alpha,alpha-trifluoroanisole

Chemical Property:

• PSA: 9.23000
• LogP: 3.95230

Purity/Quality:

97% ^*data from raw suppliers

4-Bromo-2-iodo-1-(trifluoromethoxy)benzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Bromo-2-iodophenyl trifluoromethyl ether, 4-Bromo-2-iodo-alpha,alpha,alpha-trifluoroanisole

There total 1 articles about 4-Bromo-2-iodophenyl trifluoromethyl ether, 4-Bromo-2-iodo-alpha,alpha,alpha-trifluoroanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

5-bromo-2-(trifluoromethoxy)aniline (886762-08-9) → 4-bromo-2-iodo-1-(trifluoromethoxy)benzene (154065-33-5)

Guidance literature:

With copper(l) iodide; tert.-butylnitrite; In acetonitrile; at 60 ℃; for 1h;

Reference yield: 42.0%

2-chloro-N-methoxy-N-methylacetamide (67442-07-3) + 4-bromo-2-iodo-1-(trifluoromethoxy)benzene (154065-33-5) → 1-(5-bromo-2-(trifluoromethoxy)phenyl)-2-chloroethan-1-one

Guidance literature:

4-bromo-2-iodo-1-(trifluoromethoxy)benzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.333333h;

2-chloro-N-methoxy-N-methylacetamide; In tetrahydrofuran; at -78 ℃; for 1h;

DOI:10.7554/eLife.54712

Reference yield:

4-bromo-2-iodo-1-(trifluoromethoxy)benzene (154065-33-5) + 4-methoxy-benzaldehyde (123-11-5) → C15H12BrF3O3 (1181682-10-9)

Guidance literature:

4-bromo-2-iodo-1-(trifluoromethoxy)benzene; With n-butyllithium; In tetrahydrofuran; toluene; at -78 ℃; for 0.333333h; Inert atmosphere;

4-methoxy-benzaldehyde; In tetrahydrofuran; toluene; at -78 ℃; for 1h;

With ammonium chloride; In tetrahydrofuran; ethyl acetate; toluene;

upstream raw materials:

5-bromo-2-(trifluoromethoxy)aniline

Downstream raw materials:

C₁₅H₁₂BrF₃O₃

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