2-Methyl-N-[(trimethylsilyl)methyl]-2-propanamine

Base Information

• Chemical Name: 2-Methyl-N-[(trimethylsilyl)methyl]-2-propanamine
• CAS No.: 79250-80-9
• Molecular Formula: C8H21NSi
• Molecular Weight: 159.347
• Mol file: 79250-80-9.mol

Synonyms:2-Methyl-N-[(trimethylsilyl)methyl]-2-propanamine;2-methyl-N-((trimethylsilyl)methyl)propan-2-amine

Chemical Property of 2-Methyl-N-[(trimethylsilyl)methyl]-2-propanamine

Chemical Property:

• Vapor Pressure: 3.04mmHg at 25°C
• Boiling Point: 155.3°C at 760 mmHg
• PKA: 10.30±0.29(Predicted)
• Flash Point: 47.7°C
• PSA: 12.03000
• Density: 0.776g/cm³
• LogP: 3.06110

Purity/Quality:

98%min ^*data from raw suppliers

2-Methyl-N-[(trimethylsilyl)methyl]-2-propanamine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Methyl-N-[(trimethylsilyl)methyl]-2-propanamine

There total 4 articles about 2-Methyl-N-[(trimethylsilyl)methyl]-2-propanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

tert-butylamine (75-64-9) + Chloromethyltrimethylsilane (2344-80-1) → N-tert-butyl<(trimethylsilyl)metyl>amine (79250-80-9)

Guidance literature:

tert-butylamine; Chloromethyltrimethylsilane; at 200 ℃; for 18h;

With sodium hydroxide; In water;

Reference yield: 72.0%

iodo(trimethylsilyl)methane (4206-67-1) + tert-butylamine (75-64-9) → N-tert-butyl<(trimethylsilyl)metyl>amine (79250-80-9)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃; for 12h;

DOI:10.1039/c6ob02069k

Reference yield:

C8H21NSi*ClH (1135084-10-4) → N-tert-butyl<(trimethylsilyl)metyl>amine (79250-80-9)

Guidance literature:

With sodium hydroxide; In water; for 1h;

upstream raw materials:

iodo(trimethylsilyl)methane

tert-butylamine

Chloromethyltrimethylsilane

C₈H₂₁NSi*ClH

Downstream raw materials:

N-tert-butyl-N-<(trimethylsilyl)methyl>benzylamine

methyl (3S,4R)-1-tert-butyl-4-(2,4-difluorophenyl)-pyrrolidine-3-carboxylate

methyl (3R,4S)-1-tert-butyl-4-(2,4-difluorophenyl)pyrrolidine-3-carboxylate

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