Cyclohexanone, 3-ethenyl-4-(1-methylethyl)-, (3S-trans)- (9CI)

Base Information

• Chemical Name: Cyclohexanone, 3-ethenyl-4-(1-methylethyl)-, (3S-trans)- (9CI)
• CAS No.: 129215-01-6
• Molecular Formula: C₁₁H₁₈O
• Molecular Weight: 166.263
• Mol file: 129215-01-6.mol

Synonyms:Cyclohexanone, 3-ethenyl-4-(1-methylethyl)-, (3S-trans)- (9CI)

Chemical Property of Cyclohexanone, 3-ethenyl-4-(1-methylethyl)-, (3S-trans)- (9CI)

Chemical Property:

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Technology Process of Cyclohexanone, 3-ethenyl-4-(1-methylethyl)-, (3S-trans)- (9CI)

There total 2 articles about Cyclohexanone, 3-ethenyl-4-(1-methylethyl)-, (3S-trans)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-(-)-4-isopropylcyclohex-2-enone (100295-52-1) + vinyl magnesium bromide (1826-67-1) → 3-ethenyl-4-isopropyl-1-<(trimethylsilyl)oxy>cyclohexene (129184-99-2) + 3-ethenyl-4-isopropylcyclohexanone (129215-01-6)

Guidance literature:

With chloro-trimethyl-silane; copper(I) bromide dimethylsulfide complex; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C, 30 min, 2.) -78 deg C, 2h;

DOI:10.1002/hlca.19900730314

Reference yield:

chloro-trimethyl-silane (75-77-4) + (S)-(-)-4-isopropylcyclohex-2-enone (100295-52-1) + vinyl magnesium bromide (1826-67-1) → 3-ethenyl-4-isopropyl-1-<(trimethylsilyl)oxy>cyclohexene (129184-99-2) + 3-ethenyl-4-isopropylcyclohexanone (129215-01-6)

Guidance literature:

With copper(I) bromide dimethylsulfide complex; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, -78 deg C, 30 min, 2.) -78 deg C, 2h;

DOI:10.1002/hlca.19900730314

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 3-ethenyl-4-isopropylcyclohexanone (129215-01-6) → ((1S,2S)-2-Isopropyl-5-oxo-cyclohexyl)-acetic acid methyl ester

Guidance literature:

Multistep reaction;

DOI:10.1021/ja00326a028

upstream raw materials:

chloro-trimethyl-silane

(S)-(-)-4-isopropylcyclohex-2-enone

vinyl magnesium bromide

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