(2S,6S)-2,6-DIALLYL-4-METHYL-1,2,3,6-TETRAHYDROPYRIDINE

Base Information

Chemical Name:(2S,6S)-2,6-DIALLYL-4-METHYL-1,2,3,6-TETRAHYDROPYRIDINE
CAS No.:157056-58-1
Molecular Formula:C₁₂H₁₉N
Molecular Weight:177.29
Hs Code.:
Mol file:157056-58-1.mol

Synonyms:(2S,6S)-2,6-DIALLYL-4-METHYL-1,2,3,6-TETRAHYDROPYRIDINE;(2S,6S)-2,6-diallyl-4-methyl-1,2,3,6-tetrahydropyridine(SALTDATA: FREE)

Suppliers and Price of (2S,6S)-2,6-DIALLYL-4-METHYL-1,2,3,6-TETRAHYDROPYRIDINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
rac-(2S,6S)-2,6-Diallyl-4-methyl-1,2,3,6-tetrahydropyridine
10mg
$ 45.00

Biosynth Carbosynth
(2S,6S)-2,6-Diallyl-4-methyl-1,2,3,6-tetrahydropyridine
5 g
$ 358.00

Biosynth Carbosynth
(2S,6S)-2,6-Diallyl-4-methyl-1,2,3,6-tetrahydropyridine
2 g
$ 179.00

Biosynth Carbosynth
(2S,6S)-2,6-Diallyl-4-methyl-1,2,3,6-tetrahydropyridine
1 g
$ 105.00

Biosynth Carbosynth
(2S,6S)-2,6-Diallyl-4-methyl-1,2,3,6-tetrahydropyridine
500 mg
$ 60.00

Biosynth Carbosynth
(2S,6S)-2,6-Diallyl-4-methyl-1,2,3,6-tetrahydropyridine
10 g
$ 609.00

American Custom Chemicals Corporation
(2S,6S)-2,6-DIALLYL-4-METHYL-1,2,3,6-TETRAHYDROPYRIDINE 95.00%
5MG
$ 500.74

Total 5 raw suppliers

Chemical Property of (2S,6S)-2,6-DIALLYL-4-METHYL-1,2,3,6-TETRAHYDROPYRIDINE

Chemical Property:

Vapor Pressure:0.0452mmHg at 25°C
Boiling Point:237.3°C at 760 mmHg
Flash Point:91.1°C
PSA：12.03000
Density:0.835g/cm³
LogP:3.14420

Purity/Quality:

98% ^*data from raw suppliers

rac-(2S,6S)-2,6-Diallyl-4-methyl-1,2,3,6-tetrahydropyridine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2S,6S)-2,6-DIALLYL-4-METHYL-1,2,3,6-TETRAHYDROPYRIDINE

There total 5 articles about (2S,6S)-2,6-DIALLYL-4-METHYL-1,2,3,6-TETRAHYDROPYRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 157056-58-1,436088-93-6
trans-2,6-diallyl-4-methyl-1,2,3,6-tetrahydropyridine

: 688-61-9,53588-88-8,90721-85-0,151452-33-4,151452-35-6
Triallylborane

: 157056-58-1,436088-93-6
cis-2,6-diallyl-4-methyl-1,2,3,6-tetrahydropyridine

Guidance literature:: at 130 ℃; for 5h;
DOI:10.1002/ejoc.200500560

Reference yield: 76.0%

: 108-89-4
picoline

: 688-61-9,53588-88-8,90721-85-0,151452-33-4,151452-35-6
Triallylborane

: 157056-58-1,436088-93-6
trans-2,6-diallyl-4-methyl-1,2,3,6-tetrahydropyridine

Guidance literature:: picoline; Triallylborane; at -30 ℃; for 0.166667h;

With isopropyl alcohol; for 2h; Heating;
DOI:10.1002/ejoc.200500560

Reference yield:

: 108-89-4
picoline

: 688-61-9,53588-88-8,90721-85-0,151452-33-4,151452-35-6
Triallylborane

: 157056-58-1,436088-93-6
trans-2,6-diallyl-4-methyl-1,2,3,6-tetrahydropyridine

: 157056-58-1,436088-93-6
cis-2,6-diallyl-4-methyl-1,2,3,6-tetrahydropyridine

Guidance literature:: picoline; Triallylborane; at -30 - 0 ℃; Inert atmosphere;

With isopropyl alcohol; at 50 ℃; for 2h; Inert atmosphere;

With sodium hydroxide; In water; Overall yield = 91 %; Inert atmosphere;
DOI:10.1007/s11172-018-2080-0