Diphenylphosphinodithioic acid cyanomethyl ester

Base Information

• Chemical Name: Diphenylphosphinodithioic acid cyanomethyl ester
• CAS No.: 24625-61-4
• Molecular Formula: C14H12NPS2
• Molecular Weight: 289.36
• Mol file: 24625-61-4.mol

Synonyms:Diphenylphosphinodithioic acid cyanomethyl ester

Chemical Property of Diphenylphosphinodithioic acid cyanomethyl ester

Chemical Property:

• Melting Point: 78 - 79.5 °C (hexane)
• PSA: 90.99000
• LogP: 3.93928

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Diphenylphosphinodithioic acid cyanomethyl ester

There total 2 articles about Diphenylphosphinodithioic acid cyanomethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

sodium diphenylphosphinodithioate (5827-17-8) + chloroacetonitrile (107-14-2) → (diphenylphosphinothioylthio)acetonitrile (24625-61-4)

Guidance literature:

With pyrographite; In methanol; for 72h;

Reference yield: 16.0%

diphenylphosphinodithioic acid (1015-38-9) + chloroacetonitrile (107-14-2) → 2-chlorothioacetamide (73392-36-6) + (diphenylphosphinothioylthio)acetonitrile (24625-61-4) + diphenylthiophosphinoyl chloride (1015-37-8)

Guidance literature:

In benzene; for 1200h;

upstream raw materials:

sodium diphenylphosphinodithioate

chloroacetonitrile

diphenylphosphinodithioic acid

Refernces