Ethyl 2,3-dichlorobenzoate

Base Information

Chemical Name:Ethyl 2,3-dichlorobenzoate
CAS No.:31273-66-2
Molecular Formula:C9H8Cl2O2
Molecular Weight:219.067
Hs Code.:2916399090
DSSTox Substance ID:DTXSID20604807
Nikkaji Number:J2.307.151G
Wikidata:Q82502833
Mol file:31273-66-2.mol

Synonyms:Ethyl 2,3-dichlorobenzoate;31273-66-2;Ethyl 2,3-dichloro benzoate;2,3-Dichloro-benzoic acid ethyl ester;Ethyl2,3-dichlorobenzoate;ethyl-2,3-dichlorobenzoate;SCHEMBL11418791;DTXSID20604807;MFCD06204334;AKOS008947759;DB-024678;J-520665

Suppliers and Price of Ethyl 2,3-dichlorobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
2,3-Dichloro-benzoicacidethylester 95%+
1g
$ 342.00

Crysdot
Ethyl2,3-dichlorobenzoate 95+%
25g
$ 579.00

AHH
ethyl2,3-dichlorobenzoate 97%
1g
$ 235.00

Advanced Chemicals Intermediatesced Chemicals Intermediates
2,3-Dichloro-benzoicacidethylester 95%+
10g
$ 855.50

Acints
2,3-Dichloro-benzoicacidethylester 95%+
10g
$ 855.50

Acints
2,3-Dichloro-benzoicacidethylester 95%+
5g
$ 485.75

Acints
2,3-Dichloro-benzoicacidethylester 95%+
1g
$ 137.75

Total 6 raw suppliers

Chemical Property of Ethyl 2,3-dichlorobenzoate

Chemical Property:

Melting Point:90-92 °C
Boiling Point:285.8±20.0 °C(Predicted)
PSA：26.30000
Density:1.305±0.06 g/cm3(Predicted)
LogP:3.17010
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:217.9901349
Heavy Atom Count:13
Complexity:185

Purity/Quality:

99% ^*data from raw suppliers

2,3-Dichloro-benzoicacidethylester 95%+ ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)C1=C(C(=CC=C1)Cl)Cl

Technology Process of Ethyl 2,3-dichlorobenzoate

There total 2 articles about Ethyl 2,3-dichlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: C₁₅H₂₁Cl₂MgN

: 541-41-3
chloroformic acid ethyl ester

: 31273-66-2
ethyl 2,3-dichlorobenzoate

Guidance literature:: C₁₅H₂₁Cl₂MgN; With zinc(II) chloride; In tetrahydrofuran; at 0 ℃; for 0.166667h; Inert atmosphere;

chloroformic acid ethyl ester; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 25 ℃; for 3h; Inert atmosphere;
DOI:10.1002/adsc.201300185

Reference yield:

: 64-17-5
ethanol

: 50-45-3
2,3-dichlorbenzoic acid

: 31273-66-2
ethyl 2,3-dichlorobenzoate

Guidance literature:: With sulfuric acid; for 3h; Heating;
DOI:10.1016/j.ejmech.2006.03.002

Reference yield: 73.0%

: 31273-66-2
ethyl 2,3-dichlorobenzoate

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: ethyl 2,3-dichloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

Guidance literature:: With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine; at 80 ℃; for 18h; regioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1055/s-0037-1610538