1-(2-METHOXY-4,6-DIMETHYLPYRIDIN-3-YL)METHANAMINE

Base Information

• Chemical Name: 1-(2-METHOXY-4,6-DIMETHYLPYRIDIN-3-YL)METHANAMINE
• CAS No.: 46002-83-9
• Molecular Formula: C₉H₁₄N₂O
• Molecular Weight: 166.223
• Hs Code.: 2933399090
• Mol file: 46002-83-9.mol

Synonyms:1-(2-METHOXY-4,6-DIMETHYLPYRIDIN-3-YL)METHANAMINE;1-(2-methoxy-4,6-dimethylpyridin-3-yl)methanamine(SALTDATA: FREE);(2-Methoxy-4,6-diMethylpyridin-3-yl)MethanaMine

Chemical Property of 1-(2-METHOXY-4,6-DIMETHYLPYRIDIN-3-YL)METHANAMINE

Chemical Property:

• Vapor Pressure: 0.00806mmHg at 25°C
• Boiling Point: 267.6°C at 760 mmHg
• Flash Point: 115.7°C
• PSA: 48.14000
• Density: 1.044g/cm³
• LogP: 1.86600

Purity/Quality:

97% ^*data from raw suppliers

1-(2-methoxy-4,6-dimethyl-3-pyridinyl)methanamine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: T
• Statements: 25
• Safety Statements: 45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(2-METHOXY-4,6-DIMETHYLPYRIDIN-3-YL)METHANAMINE

There total 5 articles about 1-(2-METHOXY-4,6-DIMETHYLPYRIDIN-3-YL)METHANAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

3-cyano-4,6-dimethyl-2-methoxypyridine (65515-39-1) → 1-(2-methoxy-4,6-dimethylpyridin-3-yl)methanamine (46002-83-9)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 20 ℃; for 21.5h; Cooling with ice;

Reference yield:

2-chloro-4,6-dimethylnicotinonitrile (14237-71-9) → 1-(2-methoxy-4,6-dimethylpyridin-3-yl)methanamine (46002-83-9) + 3-cyano-4,6-dimethyl-2-methoxypyridine (65515-39-1)

Guidance literature:

Reference yield:

2-chloro-4,6-dimethylnicotinonitrile (14237-71-9) → 1-(2-methoxy-4,6-dimethylpyridin-3-yl)methanamine (46002-83-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium / 4 h / 70 °C

2: lithium aluminium tetrahydride; tert-butyl methyl ether / tetrahydrofuran / 1 h / 20 °C

With lithium aluminium tetrahydride; tert-butyl methyl ether; sodium; In tetrahydrofuran;

upstream raw materials:

3-cyano-4,6-dimethyl-2-methoxypyridine

2-chloro-4,6-dimethylnicotinonitrile

3-Cyano-4,6-dimethyl-2(1H)-pyridon

Downstream raw materials:

methyl 3-bromo-6-(2-{[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]amino}ethoxy)-2-methylbenzoate

methyl 2-(2-{[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]amino}ethoxy)-3-(propan-2-yloxy)benzoate

(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methylamine hydrochloride

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