2-broMo-6-(trifluoroMethyl)pyridine-3-carbaldehyde

Base Information

• Chemical Name: 2-broMo-6-(trifluoroMethyl)pyridine-3-carbaldehyde
• CAS No.: 1192263-89-0
• Molecular Formula: C₇H₃BrF₃NO
• Molecular Weight: 254.006
• Hs Code.: 2933399990
• Mol file: 1192263-89-0.mol

Synonyms:2-broMo-6-(trifluoroMethyl)pyridine-3-carbaldehyde;2-Bromo-6-(trifluoromethyl)nicotinaldehyde 85+%;2-Bromo-6-(trifluoromethyl)pyridine-3-carboxaldehyde, 2-Bromo-3-formyl-6-(trifluoromethyl)pyridine

Chemical Property of 2-broMo-6-(trifluoroMethyl)pyridine-3-carbaldehyde

Chemical Property:

• Boiling Point: 245.8±40.0 °C(Predicted)
• PKA: -5.70±0.22(Predicted)
• PSA: 29.96000
• Density: 1.763±0.06 g/cm3(Predicted)
• LogP: 2.67540
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2-Bromo-6-(trifluoromethyl)nicotinaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-broMo-6-(trifluoroMethyl)pyridine-3-carbaldehyde

There total 1 articles about 2-broMo-6-(trifluoroMethyl)pyridine-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-bromo-6-(trifluoromethyl)pyridine (189278-27-1) + formic acid ethyl ester (109-94-4) → 2-bromo-6-trifluoromethyl-3-pyridinecarboxaldehyde (1192263-89-0)

Guidance literature:

2-bromo-6-(trifluoromethyl)pyridine; With n-butyllithium; isopropylamine; In tetrahydrofuran; hexane; at -90 - 40 ℃; for 2h;

formic acid ethyl ester; In tetrahydrofuran; hexane; at 20 ℃; for 9h;

With hydrogenchloride; In tetrahydrofuran; hexane; water;

Reference yield: 52.0%

2-bromo-6-trifluoromethyl-3-pyridinecarboxaldehyde (1192263-89-0) → (2-bromo-6-(trifluoromethyl)pyridin-3-yl)methanol (888738-18-9)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; at 0 ℃; for 12h;

upstream raw materials:

2-bromo-6-(trifluoromethyl)pyridine

formic acid ethyl ester

Downstream raw materials:

(2-bromo-6-(trifluoromethyl)pyridin-3-yl)methanol

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