2,3-dihydro-5-methoxy-6-Benzofurancarboxaldehyde

Base Information

Chemical Name:2,3-dihydro-5-methoxy-6-Benzofurancarboxaldehyde
CAS No.:99355-75-6
Molecular Formula:C₁₀H₁₀O₃
Molecular Weight:178.188
Hs Code.:
Mol file:99355-75-6.mol

Synonyms:2,3-dihydro-5-methoxy-6-Benzofurancarboxaldehyde;5-methoxy-2,3-dihydrobenzofuran-6-carbaldehyde

Suppliers and Price of 2,3-dihydro-5-methoxy-6-Benzofurancarboxaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-METHOXY-2,3-DIHYDRO-1-BENZOFURAN-6-CARBALDEHYDE 95.00%
5MG
$ 500.56

Total 1 raw suppliers

Chemical Property of 2,3-dihydro-5-methoxy-6-Benzofurancarboxaldehyde

Chemical Property:

PSA：35.53000
LogP:1.44260

Purity/Quality:

97% ^*data from raw suppliers

5-METHOXY-2,3-DIHYDRO-1-BENZOFURAN-6-CARBALDEHYDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3-dihydro-5-methoxy-6-Benzofurancarboxaldehyde

There total 15 articles about 2,3-dihydro-5-methoxy-6-Benzofurancarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 40492-54-4
6-bromo-5-methoxy-2,3-dihydro-benzofuran

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 99355-75-6
5-methoxy-2,3-dihydrobenzofuran-6-carboxaldehyde

Guidance literature:: 6-bromo-5-methoxy-2,3-dihydro-benzofuran; With n-butyllithium; In tetrahydrofuran; at -25 ℃;

N,N-dimethyl-formamide; In tetrahydrofuran; at -25 ℃;
DOI:10.1016/S0040-4039(00)00159-3

Reference yield: 41.0%

: 13391-30-5
2,3-dihydro-5-methoxybenzofuran

: 4885-02-3
Dichloromethyl methyl ether

: 99355-75-6
5-methoxy-2,3-dihydrobenzofuran-6-carboxaldehyde

Guidance literature:: With titanium tetrachloride; In dichloromethane; for 1.5h; Ambient temperature;

Reference yield:

: 150-76-5
4-methoxy-phenol

: 99355-75-6
5-methoxy-2,3-dihydrobenzofuran-6-carboxaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: BCl₃, AlCl₃ / CH₂Cl₂; 1,2-dichloro-ethane / 2.5 h

2: AcONa / methanol / 1.5 h / Heating

3: 99 percent / H₂ / 20percent palladium hydroxide / ethanol / 2280 Torr

4: 41 percent / TiCl₄ / CH₂Cl₂ / 1.5 h / Ambient temperature

With aluminium trichloride; hydrogen; sodium acetate; boron trichloride; titanium tetrachloride; palladium dihydroxide; In methanol; ethanol; dichloromethane; 1,2-dichloro-ethane;