6,6-dichlorofulvene

Base Information

Chemical Name:6,6-dichlorofulvene
CAS No.:35310-97-5
Molecular Formula:C₆H₄Cl₂
Molecular Weight:147.004
Hs Code.:
Mol file:35310-97-5.mol

Synonyms:6,6-dichlorofulvene

Suppliers and Price of 6,6-dichlorofulvene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 44 raw suppliers

Chemical Property of 6,6-dichlorofulvene

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6,6-dichlorofulvene

There total 1 articles about 6,6-dichlorofulvene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-66-3,8013-54-5
chloroform

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 95-49-8
2-methylchlorobenzene

: 95-57-8
2-monochlorophenol

: 32252-45-2
6-chlorofulvene

: 35310-97-5
6,6-dichlorofulvene

Guidance literature:: With oxygen; Further byproducts given. Title compound not separated from byproducts; Formation of xenobiotics; combustion;
DOI:10.1016/S0045-6535(00)00216-2

Reference yield:

: 35310-97-5
6,6-dichlorofulvene

: benzovindiflupyr

Guidance literature:: Multi-step reaction with 6 steps

1.1: aluminum (III) chloride / tetrahydrofuran / 5 h / -9 °C / Inert atmosphere

1.2: 0.5 h / -9 °C

2.1: hydrogen / rhodium contaminated with carbon / water; tetrahydrofuran / 7 h

3.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 1.5 h / 0 - 5 °C

4.1: sulfuric acid / 0.67 h / 20 °C

5.1: hydroxylamine hydrochloride; pyridine / ethanol / 4 h / 20 °C

6.1: triethylamine / 1,4-dioxane / 3 h / 25 - 82 °C

6.2: 0.5 h

With pyridine; methanol; sodium tetrahydroborate; sulfuric acid; hydroxylamine hydrochloride; hydrogen; triethylamine; aluminum (III) chloride; rhodium contaminated with carbon; In tetrahydrofuran; 1,4-dioxane; ethanol; water;

Reference yield:

: 35310-97-5
6,6-dichlorofulvene

: 3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid (9-dichloromethylene-1,2,3,4-tetrahydro-1,4-methano-naphthalen-5-yl)amide

Guidance literature:: Multi-step reaction with 6 steps

1: aluminum (III) chloride / toluene; tetrahydrofuran / 5 h / -9 °C / Inert atmosphere

2: hydrogen / 5% Rh/C / water; tetrahydrofuran / 7 h / Inert atmosphere

3: sodium tetrahydroborate / tetrahydrofuran; methanol / 1.5 h / 0 - 5 °C

4: sulfuric acid / 0.67 h / 20 °C

5: hydroxylamine hydrochloride; pyridine / ethanol / 4 h / 20 °C

6: triethylamine / 1,4-dioxane / 3 h / 82 °C

With pyridine; sodium tetrahydroborate; sulfuric acid; hydroxylamine hydrochloride; hydrogen; triethylamine; aluminum (III) chloride; 5% Rh/C; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water; toluene; 1: Diels-Alder Reaction;