9,10-Dihydro-9,10-dioxoanthracene-1-carboxylic acid methyl ester

Base Information

Chemical Name:9,10-Dihydro-9,10-dioxoanthracene-1-carboxylic acid methyl ester
CAS No.:32114-46-8
Molecular Formula:C₁₆H₁₀O₄
Molecular Weight:266.253
Hs Code.:2918300090
Mol file:32114-46-8.mol

Synonyms:9,10-Dihydro-9,10-dioxo-1-anthracenecarboxylic acid methyl ester;9,10-Dihydro-9,10-dioxoanthracene-1-carboxylic acid methyl ester

Suppliers and Price of 9,10-Dihydro-9,10-dioxoanthracene-1-carboxylic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 9,10-Dihydro-9,10-dioxoanthracene-1-carboxylic acid methyl ester

Chemical Property:

Boiling Point:457.1±34.0 °C(Predicted)
PSA：60.44000
Density:1.351±0.06 g/cm3(Predicted)
LogP:2.24860

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 9,10-Dihydro-9,10-dioxoanthracene-1-carboxylic acid methyl ester

There total 5 articles about 9,10-Dihydro-9,10-dioxoanthracene-1-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.7%

: 187808-48-6
methyl 5-(N,N-dimethylamino)-2,4-pentadienoate

: 130-15-4
[1,4]naphthoquinone

: 32114-46-8
methyl 9,10-anthraquinone-1-carboxylate

Guidance literature:: In xylene; for 0.5h; Ambient temperature;
DOI:10.1248/cpb.45.243

Reference yield: 61.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 82-44-0
1-chloroanthracene-9,10-dione

: 32114-46-8
methyl 9,10-anthraquinone-1-carboxylate

Guidance literature:: With dichloro[2,2'-bis(diphenylphosphino)-1,1'-binaphthyl]palladium(II); triethylamine; at 100 ℃; for 18h; under 2585.74 Torr;
DOI:10.1021/ol0498287

Reference yield:

: 623-43-8
crotonic acid methyl ester

: 32114-46-8
methyl 9,10-anthraquinone-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 71.2 percent / 4 h / 150 °C

2: 66.7 percent / xylene / 0.5 h / Ambient temperature

In xylene;
DOI:10.1248/cpb.45.243