N-(3-Methoxyphenyl)formamide

Base Information

• Chemical Name: N-(3-Methoxyphenyl)formamide
• CAS No.: 27153-17-9
• Molecular Formula: C₈H₉NO₂
• Molecular Weight: 151.165
• Mol file: 27153-17-9.mol

Synonyms:3'-Methoxyformanilide;N-(3-Methoxyphenyl)formamide;META-FORMANISIDIDE

Chemical Property of N-(3-Methoxyphenyl)formamide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

META-FORMANISIDIDE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(3-Methoxyphenyl)formamide

There total 25 articles about N-(3-Methoxyphenyl)formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-chlorophenyl formate (1988-22-3) + m-Anisidine (536-90-3,918666-97-4) → 3-Methoxy-formanilid (27153-17-9)

Guidance literature:

In neat (no solvent); at 20 ℃; for 2h;

DOI:10.1080/00397911.2016.1255334

Reference yield: 95.0%

m-Anisidine (536-90-3,918666-97-4) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 3-Methoxy-formanilid (27153-17-9)

Guidance literature:

With [2,2]bipyridinyl; boron trifluoride diethyl etherate; oxygen; palladium diacetate; Trimethylacetic acid; In toluene; at 120 ℃; for 24h;

DOI:10.1016/j.tet.2015.10.008

Reference yield: 94.0%

formic acid (64-18-6) + m-Anisidine (536-90-3,918666-97-4) → 3-Methoxy-formanilid (27153-17-9)

Guidance literature:

With zinc(II) oxide; In water; at 70 ℃; for 0.1h; chemoselective reaction; Green chemistry;

DOI:10.1080/15533174.2012.741180

upstream raw materials:

formic acid

m-Anisidine

1-(m-methoxyphenyl)-4,5-dihydro-5-hydroxy-1H-1,2,3-triazole

diethyl (3-methoxybenzoyl)phosphonate

Downstream raw materials:

m-Methoxythioformanilid

3-methoxy-N-methylaniline

3-methoxyphenyl isothiocyanate

(3-methoxy)phenylisonitrile