Technology Process of Cyclohexaneacetic acid, 4-[4-[6-(aMinocarbonyl)-3,5-diMethyl-2-pyrazinyl]phenyl]-, Methyl ester, trans-
There total 5 articles about Cyclohexaneacetic acid, 4-[4-[6-(aMinocarbonyl)-3,5-diMethyl-2-pyrazinyl]phenyl]-, Methyl ester, trans- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium phosphate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
1,2-dimethoxyethane; ethanol; water;
at 80 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trifluoroacetic acid / 1,2-dichloro-ethane / 4 h / Heating
2: trichlorophosphate / propyl cyanide / 0.17 h / 150 °C / Microwave irradiation
3: ammonia / methanol / 20 °C
4: potassium phosphate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; ethanol; water / 16 h / 80 °C
With
potassium phosphate; ammonia; trifluoroacetic acid; trichlorophosphate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
methanol; 1,2-dimethoxyethane; propyl cyanide; ethanol; water; 1,2-dichloro-ethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trichlorophosphate / propyl cyanide / 0.17 h / 150 °C / Microwave irradiation
2: ammonia / methanol / 20 °C
3: potassium phosphate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; ethanol; water / 16 h / 80 °C
With
potassium phosphate; ammonia; trichlorophosphate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
methanol; 1,2-dimethoxyethane; propyl cyanide; ethanol; water;
