Nickel(II) tetramethoxyphenylporphyrin

Base Information

• Chemical Name: Nickel(II) tetramethoxyphenylporphyrin
• CAS No.: 39828-57-4
• Molecular Formula: C48H36NiN4O4
• Molecular Weight: 791.528
• Mol file: 39828-57-4.mol

Synonyms:Nickel(II) tetramethoxyphenylporphyrin

Chemical Property of Nickel(II) tetramethoxyphenylporphyrin

Chemical Property:

• PSA: 52.80000
• LogP: 6.47220

Purity/Quality:

99%, ^*data from raw suppliers

Nickel(II)tetramethoxyphenylporphyrin 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Nickel(II) tetramethoxyphenylporphyrin

There total 3 articles about Nickel(II) tetramethoxyphenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

bis(1,5-cyclooctadiene)nickel (0) (1295-35-8) + 5,10,15,20-tetrakis(4-methoxyphenyl)porphyrin (22112-78-3) → Ni(2+)-α,β,γ,δ-tetra(4-methoxyphenyl)porphine (39828-57-4)

Guidance literature:

In toluene; at 20 ℃; for 1h; Inert atmosphere; Glovebox;

DOI:10.1021/acs.inorgchem.7b03164

Reference yield:

pyrrole (109-97-7,30604-81-0) + nickel(II) acetylacetonate (3264-82-2) + 4-methoxy-benzaldehyde (123-11-5) → [CH3OC6H4CC4H2NC(O)(CH3OC6H4)(C4H2N)]3Ni3 + Ni(2+)-α,β,γ,δ-tetra(4-methoxyphenyl)porphine (39828-57-4)

Guidance literature:

With H₂O; CF₃COOH; 2,3-dichloro-5,6-dicyano-1,4-benzoquinone; In dichloromethane; treating with CF3COOH for 2 h; oxidation with DDQ for 1 h; metallation with Ni(acac)2;

DOI:10.1002/anie.200604882

Reference yield:

5,10,15,20-meso-tetra(p-methoxyphenyl) porphyrin + nickel diacetate (373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6) → Ni(2+)-α,β,γ,δ-tetra(4-methoxyphenyl)porphine (39828-57-4)

Guidance literature:

In N,N-dimethyl-formamide; boiling DMF; 30-60 min; column chromy. (silica gel, eluant chloroform); UV;

upstream raw materials:

pyrrole

nickel(II) acetylacetonate

4-methoxy-benzaldehyde

nickel diacetate

Downstream raw materials:

nickel(II) oxide

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