N-(4-methylbenzyl)-N-(1-phenylethyl)amine

Base Information

• Chemical Name: N-(4-methylbenzyl)-N-(1-phenylethyl)amine
• CAS No.: 202199-08-4
• Molecular Formula: C₁₆H₁₉N
• Molecular Weight: 225.334
• Mol file: 202199-08-4.mol

Synonyms:N-(4-methylbenzyl)-N-(1-phenylethyl)amine;AKOS JY2033517;UKRORGSYN-BB BBV-118344;(4-methylbenzyl)(1-phenylethyl)amine(SALTDATA: HCl)

Chemical Property of N-(4-methylbenzyl)-N-(1-phenylethyl)amine

Chemical Property:

• Vapor Pressure: 0.000198mmHg at 25°C
• Boiling Point: 327.8°C at 760 mmHg
• Flash Point: 147.9°C
• Density: 1g/cm³

Purity/Quality:

98%min ^*data from raw suppliers

N-(4-Methylbenzyl)-1-phenyl-1-ethanaminehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(4-methylbenzyl)-N-(1-phenylethyl)amine

There total 7 articles about N-(4-methylbenzyl)-N-(1-phenylethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

4-methyl-benzaldehyde (104-87-0) + rac-methylbenzylamine (618-36-0) → N-(4-methylbenzyl)-1-phenylethan-1-amine (830325-12-7,202199-08-4)

Guidance literature:

With iron pentacarbonyl; In neat (no solvent); at 140 ℃; for 4h; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1039/c7ob02795h

Reference yield: 78.0%

4-Methylbenzyl alcohol (589-18-4) + rac-methylbenzylamine (618-36-0) → N-(4-methylbenzyl)-1-phenylethan-1-amine (830325-12-7,202199-08-4)

Guidance literature:

With μ-diiodo-di((η5-pentamethylcyclopentadienyl)(iodo)iridium); In water; at 115 ℃; for 10h; Inert atmosphere;

DOI:10.1039/b923083a

Reference yield:

(S)-1-phenyl-ethylamine (2627-86-3) + 4-methyl-benzaldehyde (104-87-0) → (S)-N-(4-methylbenzyl)-1-phenylethanamine (1109286-63-6,830325-12-7,202199-08-4)

Guidance literature:

(S)-1-phenyl-ethylamine; 4-methyl-benzaldehyde; In methanol; water; at 0 ℃; for 0.5h;

With borane-ammonia complex; In methanol; water; at 20 ℃; for 6h; Sealed tube;

DOI:10.1016/j.molcata.2015.08.022

upstream raw materials:

(R)-1-phenyl-ethyl-amine

4-methyl-benzaldehyde

acetophenone

para-methylbenzylamine

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