2,2,2-Trifluoro-N-phenylacetimidic Acid Benzyl Ester

Base Information

• Chemical Name: 2,2,2-Trifluoro-N-phenylacetimidic Acid Benzyl Ester
• CAS No.: 952057-61-3
• Molecular Formula: C15H12F3NO
• Molecular Weight: 279.262
• Mol file: 952057-61-3.mol

Synonyms:2,2,2-Trifluoro-N-phenylacetimidic Acid Benzyl Ester;Benzyl 2,2,2-Trifluoro-N-phenylacetimidate

Chemical Property of 2,2,2-Trifluoro-N-phenylacetimidic Acid Benzyl Ester

Chemical Property:

• Vapor Pressure: 0.002mmHg at 25°C
• Refractive Index: 1.5210-1.5250
• Boiling Point: 304.862°C at 760 mmHg
• Flash Point: 138.176°C
• PSA: 21.59000
• Density: 1.21
• LogP: 4.49570
• Storage Temp.: Refrigerator

Purity/Quality:

97% ^*data from raw suppliers

Benzyl 2,2,2-Trifluoro-N-phenylacetimidate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2,2-Trifluoro-N-phenylacetimidic Acid Benzyl Ester

There total 1 articles about 2,2,2-Trifluoro-N-phenylacetimidic Acid Benzyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2,2,2-trifluoro-N-phenyl-acetimidoyl chloride (61881-19-4) + benzyl alcohol (100-51-6,185532-71-2) → N-phenyl-2,2,2-trifluoroacetimidoyl chloride (952057-61-3)

Guidance literature:

With sodium hydride; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1246/cl.2007.992

Reference yield: 99.0%

N-phenyl-2,2,2-trifluoroacetimidoyl chloride (952057-61-3) + Cholestanol (80-97-7) → 5α-cholestan-3β-yl benzyl ether (69483-57-4,6242-21-3)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; 5 Angstroem MS; In 1,4-dioxane; at 20 ℃; for 1.5h;

DOI:10.1246/cl.2007.992

Reference yield: 95.0%

N-phenyl-2,2,2-trifluoroacetimidoyl chloride (952057-61-3) + 2-phenylethanol (60-12-8) → (2-(benzyloxy)ethyl)benzene (54894-37-0)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; 5 Angstroem MS; In 1,2-dimethoxyethane; at 20 ℃;

DOI:10.1246/cl.2007.992

upstream raw materials:

2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

benzyl alcohol

Downstream raw materials:

ethyl 6-(phenylmethoxy)hexanoate

ethyl (S)-(+)-2-benzyloxy-2-phenylacetate

(5S)-5-[(benzyloxy)methyl]dihydrofuran-2(3H)-one

(2-(benzyloxy)ethyl)benzene

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