2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine

Base Information

• Chemical Name: 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine
• CAS No.: 1269508-31-7
• Molecular Formula: C27H26BN3O2
• Molecular Weight: 435.32524
• Mol file: 1269508-31-7.mol

Synonyms:2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine

Chemical Property of 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine

Chemical Property:

• Melting Point: 204 °C
• Boiling Point: 641.3±57.0 °C(Predicted)
• PKA: 0.92±0.10(Predicted)
• PSA: 57.13000
• Density: 1.21±0.1 g/cm3(Predicted)
• LogP: 5.17180

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

• Uses: 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine can be used as an intermediate in organic synthesis, mainly used in laboratory research and development and chemical production processes.

Technology Process of 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine

There total 11 articles about 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.8%

2-(3-bromophenyl)-4,6-diphenyl-[1,3,5]triazine (864377-31-1) + bis(pinacol)diborane (73183-34-3) → 4,4,5,5-tetramethyl-2-(5'-phenyl-[1,1’:3' ,1-terphenyl]-4-yl)-1,3,2-dioxaborolane (1269508-31-7)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; for 17h; Reflux;

Reference yield: 94.0%

bis(pinacol)diborane (73183-34-3) + 3-chloro-(4,6-diphenyl-1,3,5-triazin-2-yl)benzene (307929-32-4) → 4,4,5,5-tetramethyl-2-(5'-phenyl-[1,1’:3' ,1-terphenyl]-4-yl)-1,3,2-dioxaborolane (1269508-31-7)

Guidance literature:

With potassium acetate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tricyclohexylphosphine; In 1,4-dioxane; for 10h; Inert atmosphere; Reflux;

Reference yield: 89.0%

→ 4,4,5,5-tetramethyl-2-(5'-phenyl-[1,1’:3' ,1-terphenyl]-4-yl)-1,3,2-dioxaborolane (1269508-31-7)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In N,N-dimethyl-formamide; at 150 ℃; for 48h; Inert atmosphere;

upstream raw materials:

2-(3-bromophenyl)-4,6-diphenyl-[1,3,5]triazine

bis(pinacol)diborane

3-chloro-(4,6-diphenyl-1,3,5-triazin-2-yl)benzene

bromobenzene

Downstream raw materials:

2-(3'-chloro-[1,1'-biphenyl]-3-yl)-4,6-diphenyl-1,3,5-triazine

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