Trimethyl[[(1R)-5β-methyl-2α-isopropenylcyclohexyl]oxy]silane

Base Information

Chemical Name:Trimethyl[[(1R)-5β-methyl-2α-isopropenylcyclohexyl]oxy]silane
CAS No.:57396-86-8
Molecular Formula:C13H26OSi
Molecular Weight:226.434
Hs Code.:
Mol file:57396-86-8.mol

Synonyms:Trimethyl[[(1R)-5β-methyl-2α-isopropenylcyclohexyl]oxy]silane

Suppliers and Price of Trimethyl[[(1R)-5β-methyl-2α-isopropenylcyclohexyl]oxy]silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Trimethyl[[(1R)-5β-methyl-2α-isopropenylcyclohexyl]oxy]silane

Chemical Property:

PSA：9.23000
LogP:4.21880

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Trimethyl[[(1R)-5β-methyl-2α-isopropenylcyclohexyl]oxy]silane

There total 6 articles about Trimethyl[[(1R)-5β-methyl-2α-isopropenylcyclohexyl]oxy]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 75-77-4
chloro-trimethyl-silane

: 7786-67-6,18674-65-2,20549-46-6,21290-09-5,29141-10-4,50373-36-9,59905-53-2,59905-54-3,96612-21-4,104870-56-6,121468-66-4,122517-60-6,122517-61-7,144541-38-8,89-79-2
isopulegol

: 57396-86-8
C₁₃H₂₆OSi

Guidance literature:: With 1H-imidazole; dmap; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1002/ejoc.200700904

Reference yield:

: C₁₃H₂₇IOSi

: 57396-86-8
C₁₃H₂₆OSi

Guidance literature:: With 1-(diphenylphosphino)ferrocene-1-(di-tert-butylphosphino)ferrocene; palladium diacetate; caesium carbonate; In benzene; at 20 ℃; for 24h; Reagent/catalyst; regioselective reaction; Inert atmosphere; Glovebox; Irradiation;
DOI:10.1021/jacs.7b08459

Reference yield:

: 2216-51-5
(-)-menthol

: 57396-86-8
C₁₃H₂₆OSi

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / acetonitrile / 20 °C / Inert atmosphere

2: sodium iodide / acetonitrile / 85 °C / Inert atmosphere

3: palladium diacetate; caesium carbonate; 1-(diphenylphosphino)ferrocene-1-(di-tert-butylphosphino)ferrocene / benzene / 24 h / 20 °C / Inert atmosphere; Glovebox; Irradiation

With 1H-imidazole; 1-(diphenylphosphino)ferrocene-1-(di-tert-butylphosphino)ferrocene; palladium diacetate; caesium carbonate; sodium iodide; In acetonitrile; benzene; 2: |Finkelstein Reaction;
DOI:10.1021/jacs.7b08459