2-(Diethoxymethyl)acrylonitrile

Base Information Edit

Chemical Name:2-(Diethoxymethyl)acrylonitrile
CAS No.:34450-86-7
Molecular Formula:C₈H₁₃NO₂
Molecular Weight:155.197
Hs Code.:
Mol file:34450-86-7.mol

Synonyms:2-(Diethoxymethyl)acrylonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(Diethoxymethyl)acrylonitrile Edit

Chemical Property:

PSA：42.25000
LogP:1.46528

Purity/Quality:

Safty Information:

Pictogram(s):
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Technology Process of 2-(Diethoxymethyl)acrylonitrile

There total 8 articles about 2-(Diethoxymethyl)acrylonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₃₃N₃O₂⁽²⁺⁾*2I^(1-)

: 34450-86-7
2-Diaethyoxymethyl-acrylnitril

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1007/BF02494813

Reference yield:

: 3699-12-5
3c-ethoxy-2-ethoxymethyl-acrylonitrile

: 34450-86-7
2-Diaethyoxymethyl-acrylnitril

Guidance literature:: With toluene-4-sulfonic acid; at 150 ℃;
DOI:10.1097/00005537-200203000-00031

Reference yield:

: 14444-77-0
diethyl phenyl orthoformate

: 34450-86-7
2-Diaethyoxymethyl-acrylnitril

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran / 1 h / 0 °C

1.2: 56 percent / MgBr₂ / tetrahydrofuran / -70 - 0 °C

2.1: acetone / 2 h / Heating

3.1: t-BuOK / tetrahydrofuran / 3 h / 20 °C

With potassium tert-butylate; lithium diisopropyl amide; In tetrahydrofuran; acetone; 1.1: Metallation / 1.2: Alkylation / 2.1: Methylation / 3.1: Elimination;
DOI:10.1007/BF02494813