(E)-2-(3-METHOXYPROPENYL)-4,4,5,5-TETRAMETHYL-(1,3,2)-DIOXABOROANE

Base Information

Chemical Name:(E)-2-(3-METHOXYPROPENYL)-4,4,5,5-TETRAMETHYL-(1,3,2)-DIOXABOROANE
CAS No.:934342-48-0
Molecular Formula:C₁₀H₁₉BO₃
Molecular Weight:198.07
Hs Code.:
Mol file:934342-48-0.mol

Synonyms:(E)-2-(3-METHOXYPROPENYL)-4,4,5,5-TETRAMETHYL-(1,3,2)-DIOXABOROANE

Suppliers and Price of (E)-2-(3-METHOXYPROPENYL)-4,4,5,5-TETRAMETHYL-(1,3,2)-DIOXABOROANE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of (E)-2-(3-METHOXYPROPENYL)-4,4,5,5-TETRAMETHYL-(1,3,2)-DIOXABOROANE

Chemical Property:

Refractive Index:n20/D 1.4430(lit.)
Boiling Point:229-230 °C(lit.)
Flash Point:214 °F
PSA：27.69000
Density:0.933 g/mL at 25 °C(lit.)
LogP:2.84820

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (E)-2-(3-METHOXYPROPENYL)-4,4,5,5-TETRAMETHYL-(1,3,2)-DIOXABOROANE

There total 6 articles about (E)-2-(3-METHOXYPROPENYL)-4,4,5,5-TETRAMETHYL-(1,3,2)-DIOXABOROANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 627-41-8
propargyl alcohol methyl ether

: 165059-42-7,934342-48-0
(E)-3-methoxy-1-propenylboronic acid pinacol ester

Guidance literature:: With bis(cyclohexanyl)borane; at 20 ℃; for 4h;
DOI:10.1055/s-2004-829165

Reference yield: 50.0%

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 627-41-8
propargyl alcohol methyl ether

: 165059-42-7,934342-48-0
2-(3-methoxy-propenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Guidance literature:: propargyl alcohol methyl ether; With Schwartz's reagent; at 20 ℃; for 0.5h; Sealed tube; Inert atmosphere;

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In dichloromethane-d2; at 60 ℃; Sealed tube; Inert atmosphere;

With boron trifluoride diethyl etherate; In dichloromethane-d2; at 20 ℃; for 1h; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.7b01778

Reference yield: 43.0%

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 627-41-8
propargyl alcohol methyl ether

: 126689-01-8
cyclopropylboronic acid pinacol ester

: 165059-42-7,934342-48-0
2-(3-methoxy-propenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Guidance literature:: propargyl alcohol methyl ether; With Schwartz's reagent; at 20 ℃; for 0.5h; Sealed tube; Inert atmosphere;

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In dichloromethane-d2; at 60 ℃; Sealed tube; Inert atmosphere;

With boron trifluoride diethyl etherate; In dichloromethane-d2; at 20 ℃; for 1h; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.7b01778