N-T-Butyl 2-bromobenzamide

Base Information

Chemical Name:N-T-Butyl 2-bromobenzamide
CAS No.:168265-57-4
Molecular Formula:C₁₁H₁₄BrNO
Molecular Weight:256.142
Hs Code.:2924299090
DSSTox Substance ID:DTXSID90352262
Wikidata:Q82129305
Mol file:168265-57-4.mol

Synonyms:168265-57-4;2-Bromo-N-(tert-butyl)benzamide;N-T-BUTYL 2-BROMOBENZAMIDE;2-bromo-N-tert-butylbenzamide;N-tert-butyl 2-bromobenzamide;SCHEMBL9129787;DTXSID90352262;TVNDQPPEFATMSD-UHFFFAOYSA-N;MFCD00462994;STK012694;AKOS000197863;BS-21704;CS-0196847;E73956;A882182;Z28277793

Suppliers and Price of N-T-Butyl 2-bromobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
N-t-Butyl 2-bromobenzamide
100mg
$ 305.00

TRC
N-t-Butyl2-bromobenzamide
1g
$ 75.00

TRC
N-t-Butyl2-bromobenzamide
100mg
$ 45.00

Crysdot
2-Bromo-N-(tert-butyl)benzamide 95+%
100g
$ 600.00

Aronis compounds
2-bromo-N-(tert-butyl)benzamide
20mg
$ 30.00

American Custom Chemicals Corporation
2-BROMO-N-TERT-BUTYLBENZAMIDE 95.00%
5MG
$ 503.51

AK Scientific
N-t-Butyl2-bromobenzamide
25g
$ 371.00

AK Scientific
N-t-Butyl2-bromobenzamide
1g
$ 91.00

Total 10 raw suppliers

Chemical Property of N-T-Butyl 2-bromobenzamide

Chemical Property:

Boiling Point:342.2±25.0 °C(Predicted)
PKA:14.23±0.46(Predicted)
PSA：32.59000
Density:1.309±0.06 g/cm3(Predicted)
LogP:3.55220
Storage Temp.:Sealed in dry,Room Temperature
XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:255.02588
Heavy Atom Count:14
Complexity:210

Purity/Quality:

97% ^*data from raw suppliers

N-t-Butyl 2-bromobenzamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)NC(=O)C1=CC=CC=C1Br

Technology Process of N-T-Butyl 2-bromobenzamide

There total 6 articles about N-T-Butyl 2-bromobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 540-88-5
acetic acid tert-butyl ester

: 2042-37-7
o-cyanobromobenzene

: 168265-57-4
2-bromo-N-(tert-butyl)benzamide

Guidance literature:: With toluene-4-sulfonic acid; at 80 ℃; for 3h; Reagent/catalyst; Temperature; Green chemistry;
DOI:10.1080/00304948.2016.1194126

Reference yield: 86.0%

: 75-64-9
tert-butylamine

: 88-65-3
2-bromobenzoic-acid

: 168265-57-4
2-bromo-N-(tert-butyl)benzamide

Guidance literature:: 2-bromobenzoic-acid; With triethylamine; isobutyl chloroformate; In dichloromethane; for 0.25h; Inert atmosphere; Schlenk technique;

tert-butylamine; In dichloromethane; at 0 ℃;
DOI:10.1002/ejoc.201501170

Reference yield: 73.0%

: 75-91-2
tert.-butylhydroperoxide

: 2042-37-7
o-cyanobromobenzene

: 168265-57-4
2-bromo-N-(tert-butyl)benzamide

Guidance literature:: o-cyanobromobenzene; With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at 0 ℃; for 0.166667h; Sealed tube;

tert.-butylhydroperoxide; In water; 1,2-dichloro-ethane; at 0 - 55 ℃; Sealed tube;
DOI:10.1002/adsc.201700532