PyriMidine-2-carboxiMidaMide acetate

Base Information

• Chemical Name: PyriMidine-2-carboxiMidaMide acetate
• CAS No.: 312613-82-4
• Molecular Formula: C7H10N4O2
• Molecular Weight: 182.1799
• Mol file: 312613-82-4.mol

Synonyms:PyriMidine-2-carboxiMidaMide acetate

Chemical Property of PyriMidine-2-carboxiMidaMide acetate

Chemical Property:

• PSA: 112.95000
• LogP: 0.65160
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Pyrimidine-2-carboximidamideacetate 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of PyriMidine-2-carboxiMidaMide acetate

There total 1 articles about PyriMidine-2-carboxiMidaMide acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2-cyanopyrimidine (14080-23-0) + ammonium acetate (631-61-8,92206-38-7) → 2-amidinopyrimidine acetate (312613-82-4)

Guidance literature:

In methanol; at 80 ℃; for 16h;

DOI:10.1021/acs.cgd.7b01657

Reference yield: 94.02%

2-amidinopyrimidine acetate (312613-82-4) + 2-(2-Methoxyphenoxy)propanedioic acid diethyl ester (20730-58-9) → 4,6-dihydroxy-5-(o-methoxyphenoxy)-2-(2-pyrimidinyl)-pyrimidine (329923-15-1)

Guidance literature:

With sodium methylate; In methanol; at 65 ℃; for 3h; Product distribution / selectivity;

Reference yield: 58.0%

ethyl 2-formyl-3-oxopropanoate (80370-42-9) + 2-amidinopyrimidine acetate (312613-82-4) → bipyrimidine ethyl ester (1068977-22-9)

Guidance literature:

With pyridine; at 70 ℃; for 16h; Inert atmosphere;

DOI:10.1021/acs.cgd.7b01657

upstream raw materials:

2-cyanopyrimidine

ammonium acetate

Downstream raw materials:

4,6-dihydroxy-5-(o-methoxyphenoxy)-2-(2-pyrimidinyl)-pyrimidine

bipyrimidine carboxylic acid

bipyrimidine ethyl ester

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