N-(2H-1,3-benzodioxol-5-ylmethyl)aniline

Base Information

Chemical Name:N-(2H-1,3-benzodioxol-5-ylmethyl)aniline
CAS No.:3526-42-9
Molecular Formula:C₁₄H₁₃NO₂
Molecular Weight:227.263
Hs Code.:
DSSTox Substance ID:DTXSID401277698
Nikkaji Number:J1.036.008K
Mol file:3526-42-9.mol

Synonyms:N-(2H-1,3-benzodioxol-5-ylmethyl)aniline;3526-42-9;N-(1,3-benzodioxol-5-ylmethyl)aniline;N-Phenyl-1,3-benzodioxole-5-methanamine;CBMicro_022456;ChemDiv2_000392;Oprea1_294845;Oprea1_477528;SCHEMBL9672474;DTXSID401277698;HMS1370B18;CCG-9683;AKOS000546387;N-[(1,3-dioxaindan-5-yl)methyl]aniline;BIM-0022486.P001;EU-0041327;EN300-70428;N-[(2H-1,3-benzodioxol-5-yl)methyl]aniline;Z137579684

Suppliers and Price of N-(2H-1,3-benzodioxol-5-ylmethyl)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of N-(2H-1,3-benzodioxol-5-ylmethyl)aniline

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:227.094628657
Heavy Atom Count:17
Complexity:240

Purity/Quality:: 95%, 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1OC2=C(O1)C=C(C=C2)CNC3=CC=CC=C3

Technology Process of N-(2H-1,3-benzodioxol-5-ylmethyl)aniline

There total 17 articles about N-(2H-1,3-benzodioxol-5-ylmethyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 495-76-1
piperonol

: 62-53-3
aniline

: 3526-42-9
N-(benzo[d][1,3]dioxol-5-ylmethyl)benzenamine

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; 1-mesityl-3-((1-(4-(trifluoromethyl)phenyl)-1H-1,2,3-triazol-4-yl)methyl)-1H-imidazol-3-ium bromide; potassium tert-butylate; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate; In ⁽²⁾H₈-toluene; at 100 ℃; for 6h; Inert atmosphere;
DOI:10.1021/acs.inorgchem.7b02586

Reference yield: 95.0%

: 495-76-1
piperonol

: 2325-27-1
N-phenyltriphenyliminophosphorane

: 3526-42-9
N-(benzo[d][1,3]dioxol-5-ylmethyl)benzenamine

Guidance literature:: With cesium hydroxide; palladium diacetate; In toluene; at 150 ℃; for 48h;
DOI:10.1055/s-0030-1260238

Reference yield: 93.0%

: 27738-39-2
piperonal-phenylimine

: 3526-42-9
N-(benzo[d][1,3]dioxol-5-ylmethyl)benzenamine

Guidance literature:: With ruthenium(III) chloride trihydrate; potassium carbonate; glycerol; at 130 ℃; for 24h; Inert atmosphere; Sealed tube;
DOI:10.1016/j.tet.2016.05.036