2,5-dioxo-1-Pyrrolidinepropanal

Base Information

• Chemical Name: 2,5-dioxo-1-Pyrrolidinepropanal
• CAS No.: 5615-85-0
• Molecular Formula: C₇H₉NO₃
• Molecular Weight: 155.153

Synonyms:2,5-dioxo-1-Pyrrolidinepropanal

Chemical Property of 2,5-dioxo-1-Pyrrolidinepropanal

Chemical Property:

• PSA: 54.45000
• LogP: -0.33770

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,5-dioxo-1-Pyrrolidinepropanal

There total 1 articles about 2,5-dioxo-1-Pyrrolidinepropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(prop-2-yn-1-yl)pyrrolidine-2,5-dione (10478-33-8) → 3-(2,5-dioxo-pyrrolidin-1-yl)propionaldehyde (5615-85-0) + N-(2-oxopropyl)-succinimide (30057-93-3)

Guidance literature:

With water; ruthenium-based phosphine complex; In acetone; at 120 ℃; for 72h;

DOI:10.1002/anie.200503826

Reference yield:

3-(2,5-dioxo-pyrrolidin-1-yl)propionaldehyde (5615-85-0) + Acetic acid (1R,2S,5R)-2-(1-methyl-1-phenyl-ethyl)-5-[(triphenyl-λ5-phosphanylidene)-methyl]-cyclohexyl ester → 2,2-Dimethyl-propionic acid (1R,2S,5R)-5-[(Z)-4-(2,5-dioxo-pyrrolidin-1-yl)-but-1-enyl]-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester (92845-19-7) + 2,2-Dimethyl-propionic acid (1R,2S,5R)-5-[(E)-4-(2,5-dioxo-pyrrolidin-1-yl)-but-1-enyl]-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester (92845-20-0)

Guidance literature:

In dichloromethane; for 1.33333h; Yield given. Yields of byproduct given; Ambient temperature;

DOI:10.1021/ja00338a034

Reference yield:

3-(2,5-dioxo-pyrrolidin-1-yl)propionaldehyde (5615-85-0) → 3-succinimidopropionic acid (5724-76-5)

Guidance literature:

With sodium hydroxide; potassium permanganate; water;

DOI:10.1021/ja01172a031

upstream raw materials:

1-(prop-2-yn-1-yl)pyrrolidine-2,5-dione

Downstream raw materials:

3-succinimidopropionic acid

2,2-Dimethyl-propionic acid (1R,2S,5R)-5-[(Z)-4-(2,5-dioxo-pyrrolidin-1-yl)-but-1-enyl]-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

2,2-Dimethyl-propionic acid (1R,2S,5R)-5-[(E)-4-(2,5-dioxo-pyrrolidin-1-yl)-but-1-enyl]-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

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