4-Iodo-2-methylisoquinolin-1(2H)-one

Base Information

Chemical Name:4-Iodo-2-methylisoquinolin-1(2H)-one
CAS No.:54931-61-2
Molecular Formula:C₁₀H₈INO
Molecular Weight:285.084
Hs Code.:
DSSTox Substance ID:DTXSID40481071
Wikidata:Q82316284

Synonyms:4-Iodo-2-methylisoquinolin-1(2H)-one;54931-61-2;4-IODO-2-METHYLISOQUINOLIN-1-ONE;AGN-PC-0NI4RF;SCHEMBL24271641;DTXSID40481071;4-iodo-2-methyl-1,2-dihydroisoquinolin-1-one;EN300-8332506;Z1862014185

Suppliers and Price of 4-Iodo-2-methylisoquinolin-1(2H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 4-Iodo-2-methylisoquinolin-1(2H)-one

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:284.96506
Heavy Atom Count:13
Complexity:262

Purity/Quality:: 95+% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C=C(C2=CC=CC=C2C1=O)I

Technology Process of 4-Iodo-2-methylisoquinolin-1(2H)-one

There total 1 articles about 4-Iodo-2-methylisoquinolin-1(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 5471-63-6
1,3-diphenylisobenzofuran

: 3947-77-1
2-methylisoquinolinium iodide

: 54931-61-2
4-iodo-2-methylisoquinolin-1(2H)-one

: 1159-86-0
o-dibenzoylbenzene

Guidance literature:: With sodium periodate; potassium acetate; acetic acid; In 1,2-dichloro-ethane; at 80 ℃; for 16h;
DOI:10.1021/acs.joc.0c02321

Reference yield: 94.0%

: 941-55-9
4-toluenesulfonyl azide

: 54931-61-2
4-iodo-2-methylisoquinolin-1(2H)-one

: N-(4-iodo-2-methyl-1-oxo-1,2-dihydroisoquinolin-8-yl)-4-methylbenzenesulfonamide

Guidance literature:: With silver hexafluoroantimonate; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; sodium acetate; In 1,2-dichloro-ethane; at 40 ℃; for 6h; regioselective reaction;
DOI:10.1002/adsc.201701244

Reference yield: 92.0%

: 54931-61-2
4-iodo-2-methylisoquinolin-1(2H)-one

: 536-74-3
phenylacetylene

: 54931-72-5
2-methyl-4-(phenylethynyl)isoquinolin-1(2H)-one

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 20 ℃; for 12h;
DOI:10.1002/adsc.201701244