Methyl 4-nitro-2-trifluoroMethylbenzoate

Base Information

• Chemical Name: Methyl 4-nitro-2-trifluoroMethylbenzoate
• CAS No.: 900254-47-9
• Molecular Formula: C9H6F3NO4
• Molecular Weight: 249.146
• Hs Code.: 2916399090
• Mol file: 900254-47-9.mol

Synonyms:Methyl 4-nitro-2-trifluoroMethylbenzoate

Chemical Property of Methyl 4-nitro-2-trifluoroMethylbenzoate

Chemical Property:

• Boiling Point: 309.2±42.0 °C(Predicted)
• PSA: 72.12000
• Density: 1.442±0.06 g/cm3(Predicted)
• LogP: 2.92340
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Methyl 4-nitro-2-(trifluoromethyl)benzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 4-nitro-2-trifluoroMethylbenzoate

There total 2 articles about Methyl 4-nitro-2-trifluoroMethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 4-amino-2-(trifluoromethyl)benzoic acid (393-06-6) → 4-nitro-2-trifluoromethyl benzoic acid methyl ester (900254-47-9)

Guidance literature:

With diazomethyl-trimethyl-silane; at 0 - 20 ℃;

Reference yield:

methanol (67-56-1) + 4-nitro-2-(trifluoromethyl)benzoic acid (320-37-6) → 4-nitro-2-trifluoromethyl benzoic acid methyl ester (900254-47-9)

Guidance literature:

With sulfuric acid; Heating / reflux;

Reference yield:

4-nitro-2-trifluoromethyl benzoic acid methyl ester (900254-47-9) → methyl 4-amino-2-(trifluoromethyl)benzoate (894796-87-3)

Guidance literature:

With water; tin(ll) chloride; In ethyl acetate; for 2h; Heating / reflux;

upstream raw materials:

methanol

4-nitro-2-(trifluoromethyl)benzoic acid

4-amino-2-(trifluoromethyl)benzoic acid

Downstream raw materials:

methyl 4-amino-2-(trifluoromethyl)benzoate