1-O,2-O:3-O,4-O-Diisopropylidene-5,6-dideoxy-5,6-didehydro-D-mannitol

Base Information

Chemical Name:1-O,2-O:3-O,4-O-Diisopropylidene-5,6-dideoxy-5,6-didehydro-D-mannitol
CAS No.:4239-90-1
Molecular Formula:C₁₂H₂₀O₄
Molecular Weight:228.288
Hs Code.:
Mol file:4239-90-1.mol

Synonyms:1-O,2-O:3-O,4-O-Diisopropylidene-5,6-dideoxy-5,6-didehydro-D-mannitol;3-O,4-O:5-O,6-O-Diisopropylidene-1,2-dideoxy-D-arabino-1-hexenitol;3-O,4-O:5-O,6-O-Diisopropylidene-1,2-dideoxy-D-arabino-hexa-1-enitol

Suppliers and Price of 1-O,2-O:3-O,4-O-Diisopropylidene-5,6-dideoxy-5,6-didehydro-D-mannitol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-O,2-O:3-O,4-O-Diisopropylidene-5,6-dideoxy-5,6-didehydro-D-mannitol

Chemical Property:

Purity/Quality:: 95%-98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 1-O,2-O:3-O,4-O-Diisopropylidene-5,6-dideoxy-5,6-didehydro-D-mannitol

There total 12 articles about 1-O,2-O:3-O,4-O-Diisopropylidene-5,6-dideoxy-5,6-didehydro-D-mannitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 38145-93-6
1,2:3,4-di-O-isopropylidene-D-mannitol

: 4239-90-1,22893-94-3
(4S,4'R,5R)-2,2,2',2'-tetramethyl-5-vinyl-4,4'-bi(1,3-dioxolane)

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In toluene; for 3h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2015.08.055

Reference yield: 92.0%

: 139326-94-6
1,2:3,4-di-O-isopropylidene-5,6-di-O-mesyl-D-mannitol

: 4239-90-1,22893-94-3
(4S,4'R,5R)-2,2,2',2'-tetramethyl-5-vinyl-4,4'-bi(1,3-dioxolane)

Guidance literature:: With sodium iodide; In acetone; at 100 ℃; for 6.5h;
DOI:10.1055/s-1991-28400

Reference yield: 80.0%

: 38145-93-6,58846-25-6,73745-56-9
(S)-1-((4R,4'R,5R)-2,2,2',2'-tetramethyl-4,4'-bi(1,3-dioxolan)-5-yl)ethane-1,2-diol

: 4239-90-1,22893-94-3
(4S,4'R,5R)-2,2,2',2'-tetramethyl-5-vinyl-4,4'-bi(1,3-dioxolane)

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetasy.2012.06.021