2-Naphthalenecarboxylic acid, 6-(diMethylaMino)-4-hydroxy-, Methyl ester

Base Information

• Chemical Name: 2-Naphthalenecarboxylic acid, 6-(diMethylaMino)-4-hydroxy-, Methyl ester
• CAS No.: 263026-75-1
• Molecular Formula: C14H15NO3
• Molecular Weight: 245.2738
• Hs Code.: 2922509090
• Mol file: 263026-75-1.mol

Synonyms:2-Naphthalenecarboxylic acid, 6-(diMethylaMino)-4-hydroxy-, Methyl ester;6-(Dimethylamino)-4-hydroxy-2-naphthalenecarboxylic acid methyl ester;Methyl 6-(diMethylaMino)-4-hydroxy-2-naphthoate

Chemical Property of 2-Naphthalenecarboxylic acid, 6-(diMethylaMino)-4-hydroxy-, Methyl ester

Chemical Property:

• Vapor Pressure: 2.02E-08mmHg at 25°C
• Boiling Point: 441.9°C at 760 mmHg
• Flash Point: 221.1°C
• PSA: 49.77000
• Density: 1.239
• LogP: 2.39800
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Methyl6-(dimethylamino)-4-hydroxy-2-naphthoate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Naphthalenecarboxylic acid, 6-(diMethylaMino)-4-hydroxy-, Methyl ester

There total 1 articles about 2-Naphthalenecarboxylic acid, 6-(diMethylaMino)-4-hydroxy-, Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 6-(dimethylamino)-4-hydroxy-2-naphthoic acid (31222-36-3) → methyl 6-(dimethylamino)-4-hydroxy-2-naphthoate (263026-75-1)

Guidance literature:

With sulfuric acid; for 5h; Reflux;

DOI:10.1016/j.saa.2014.10.016

Reference yield:

methyl 6-(dimethylamino)-4-hydroxy-2-naphthoate (263026-75-1) + 1,1-bis(4-methoxyphenyl)-2-propyn-1-ol (101597-25-5) → methyl 9-(dimethylamino)-2,2-bis(4-methoxyphenyl)-2H-benzo[h]chromene-5-carboxylate (214115-72-7)

Guidance literature:

With aluminum oxide; In toluene; Inert atmosphere; Reflux;

DOI:10.1016/j.saa.2014.10.016

Reference yield:

methyl 6-(dimethylamino)-4-hydroxy-2-naphthoate (263026-75-1) + 1,1-di[4,4'-bis(dimethylamino)phenyl]-2-propyn-1-ol (102164-16-9) → Methyl 9-dimethylamino-2,2-di(4-dimethylaminophenyl)-2H-naphtho[1,2-b]pyran-5-carboxylate (263026-69-3)

Guidance literature:

upstream raw materials:

methanol

6-(dimethylamino)-4-hydroxy-2-naphthoic acid

Downstream raw materials:

Methyl 9-dimethylamino-2-phenyl-2-(4-piperidinophenyl)-2H-naphtho[1,2-b]pyran-5-carboxylate

Methyl 9-dimethylamino-2,2-di(4-dimethylaminophenyl)-2H-naphtho[1,2-b]pyran-5-carboxylate

methyl 9-(dimethylamino)-2,2-bis(4-methoxyphenyl)-2H-benzo[h]chromene-5-carboxylate

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