3-(1,3-Dioxan-2-yl)-1-(4-methoxyphenyl)propan-1-one

Base Information

Chemical Name:3-(1,3-Dioxan-2-yl)-1-(4-methoxyphenyl)propan-1-one
CAS No.:121789-38-6
Molecular Formula:C14H18O4
Molecular Weight:250.295
Hs Code.:2932999099
DSSTox Substance ID:DTXSID00560179
Wikidata:Q82443177
Mol file:121789-38-6.mol

Synonyms:121789-38-6;3-(1,3-DIOXAN-2-YL)-4'-METHOXYPROPIOPHENONE;3-(1,3-Dioxan-2-yl)-1-(4-methoxyphenyl)propan-1-one;MFCD02261805;3-(1,3-DIOXAN-2-YL)-4/'-METHOXYPROPIOPHENONE;SCHEMBL1670496;DTXSID00560179;AKOS016023252;1-Propanone, 3-(1,3-dioxan-2-yl)-1-(4-methoxyphenyl)-

Suppliers and Price of 3-(1,3-Dioxan-2-yl)-1-(4-methoxyphenyl)propan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Rieke Metals
3-(1,3-dioxan-2-yl)-4'-methoxypropiophenone 97%
1g
$ 383.00

Rieke Metals
3-(1,3-dioxan-2-yl)-4'-methoxypropiophenone 97%
2g
$ 555.00

Rieke Metals
3-(1,3-DIOXAN-2-YL)-4'-METHOXYPROPIOPHENONE
1g
$ 809.00

Rieke Metals
3-(1,3-dioxan-2-yl)-4'-methoxypropiophenone 97%
5g
$ 1309.00

Rieke Metals
3-(1,3-DIOXAN-2-YL)-4'-METHOXYPROPIOPHENONE
5g
$ 1943.00

Matrix Scientific
3-(1,3-Dioxan-2-yl)-4'-methoxypropiophenone
5g
$ 1412.00

Matrix Scientific
3-(1,3-Dioxan-2-yl)-4'-methoxypropiophenone
2g
$ 688.00

Matrix Scientific
3-(1,3-Dioxan-2-yl)-4'-methoxypropiophenone
1g
$ 465.00

Crysdot
3-(1,3-Dioxan-2-yl)-4'-methoxypropiophenone 95+%
1g
$ 398.00

Crysdot
3-(1,3-Dioxan-2-yl)-4'-methoxypropiophenone 95+%
5g
$ 1360.00

Total 4 raw suppliers

Chemical Property of 3-(1,3-Dioxan-2-yl)-1-(4-methoxyphenyl)propan-1-one

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:398.268°C at 760 mmHg
Flash Point:177.107°C
PSA：44.76000
Density:1.107g/cm³
LogP:2.42110
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:250.12050905
Heavy Atom Count:18
Complexity:253

Purity/Quality:

97% ^*data from raw suppliers

3-(1,3-dioxan-2-yl)-4'-methoxypropiophenone 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C(=O)CCC2OCCCO2

Technology Process of 3-(1,3-Dioxan-2-yl)-1-(4-methoxyphenyl)propan-1-one

There total 7 articles about 3-(1,3-Dioxan-2-yl)-1-(4-methoxyphenyl)propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.1%

: 33884-43-4
2-(2-Bromoethyl)-1,3-dioxane

: 123-11-5
4-methoxy-benzaldehyde

: 121789-38-6
1-(4-Methoxyphenyl)-3-(1,3-dioxan-2-yl)-1-propanon

Guidance literature:: With ammonium chloride; magnesium; In tetrahydrofuran;

Reference yield:

: 52898-49-4
4,N-dimethoxy-N-methylbenzamide

: (1,3-dioxan-2-yl)ethylmagnesium bromide

: 121789-38-6
1-(4-Methoxyphenyl)-3-(1,3-dioxan-2-yl)-1-propanon

Guidance literature:: In tetrahydrofuran; at -78 - 20 ℃;

Reference yield:

: 121-98-2
methyl 4-methoxybenzoate

: 121789-38-6
1-(4-Methoxyphenyl)-3-(1,3-dioxan-2-yl)-1-propanon

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / KOH / methanol; H₂O / 4 h / Heating

2: thionyl chloride / 1 h / Heating

3: 1.) Mg / 1.) THF, 30 min, reflux; 2.) THF, 12 h, room temperature

With potassium hydroxide; thionyl chloride; magnesium; In methanol; water;