3-Methoxybenzoic acid phenacyl ester

Base Information

Chemical Name:3-Methoxybenzoic acid phenacyl ester
CAS No.:55153-18-9
Molecular Formula:C16H14O4
Molecular Weight:270.285
Hs Code.:
Mol file:55153-18-9.mol

Synonyms:3-Methoxybenzoic acid phenacyl ester

Suppliers and Price of 3-Methoxybenzoic acid phenacyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 3-Methoxybenzoic acid phenacyl ester

Chemical Property:

PSA：52.60000
LogP:2.73490

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-Methoxybenzoic acid phenacyl ester

There total 3 articles about 3-Methoxybenzoic acid phenacyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 586-38-9
3-Methoxybenzoic acid

: 70-11-1
α-bromoacetophenone

: 55153-18-9
2-oxo-2-phenylethyl 3-methoxybenzoate

Guidance literature:: With potassium carbonate; In methanol; water; for 15h; Heating;

Reference yield:

: 98-86-2
acetophenone

: 55153-18-9
2-oxo-2-phenylethyl 3-methoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / diethyl ether / Inert atmosphere

2: tetra-(n-butyl)ammonium iodide; potassium carbonate / dichloromethane; water / 20 °C / Inert atmosphere

With bromine; tetra-(n-butyl)ammonium iodide; potassium carbonate; In diethyl ether; dichloromethane; water;
DOI:10.1002/anie.201306231