PYRIDINE-3-BORONIC ACID DIMETHYL ESTER

Base Information

• Chemical Name: PYRIDINE-3-BORONIC ACID DIMETHYL ESTER
• CAS No.: 175885-77-5
• Molecular Formula: C7H10BNO2
• Molecular Weight: 150.973
• Mol file: 175885-77-5.mol

Synonyms:PYRIDINE-3-BORONIC ACID DIMETHYL ESTER;PYRIDINE-3-BORONIC ACID METHYL ESTER;Dimethyl (pyridin-3-yl)boronate, 3-(Dimethoxyboranyl)pyridine

Chemical Property of PYRIDINE-3-BORONIC ACID DIMETHYL ESTER

Chemical Property:

• PSA: 31.35000
• LogP: 0.06960

Purity/Quality:

99% ^*data from raw suppliers

PYRIDINE-3-BORONIC ACID DIMETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of PYRIDINE-3-BORONIC ACID DIMETHYL ESTER

There total 4 articles about PYRIDINE-3-BORONIC ACID DIMETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

methanol (67-56-1) + 3-pyridylboronic acid (1692-25-7) → pyridine-3-boronic acid dimethyl ester (175885-77-5)

Guidance literature:

at 80 ℃; for 0.5h;

DOI:10.1021/jo7018043

Reference yield: 19.0%

3-Diethylboranylpyridine (89878-14-8) → pyridine-3-boronic acid dimethyl ester (175885-77-5)

Guidance literature:

according to: M. Terashima, H. Kakimi, M. Ishikura and K. Kamata: Chem. Pharm. Bull., 31, 4573 (1983);

DOI:10.1246/bcsj.70.699

Reference yield:

3-Bromopyridine (626-55-1,163928-56-1) + n-butyllithium (109-72-8,29786-93-4) + Trimethyl borate (121-43-7,63156-11-6) → pyridine-3-boronic acid dimethyl ester (175885-77-5)

Guidance literature:

In tetrahydrofuran; hexane;

upstream raw materials:

3-Bromopyridine

n-butyllithium

Trimethyl borate

methanol

Downstream raw materials:

6-(3,4-dimethoxy-phenyl)-2-methyl-3-pyridin-3-yl-imidazo[1,2-b]pyridazine

3-pyridylboronic acid

abiraterone

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