(5S)-5-[bis[3,5-bis(trifluoroMethyl)phenyl][[(1,1-diMethylethyl)diMethylsilyl]oxy]Methyl]-2-Pyrrolidinone

Base Information

Chemical Name:(5S)-5-[bis[3,5-bis(trifluoroMethyl)phenyl][[(1,1-diMethylethyl)diMethylsilyl]oxy]Methyl]-2-Pyrrolidinone
CAS No.:1227364-30-8
Molecular Formula:C27H27F12NO2Si
Molecular Weight:653.5751184
Hs Code.:
Mol file:1227364-30-8.mol

Synonyms:(5S)-5-[bis[3,5-bis(trifluoroMethyl)phenyl][[(1,1-diMethylethyl)diMethylsilyl]oxy]Methyl]-2-Pyrrolidinone

Suppliers and Price of (5S)-5-[bis[3,5-bis(trifluoroMethyl)phenyl][[(1,1-diMethylethyl)diMethylsilyl]oxy]Methyl]-2-Pyrrolidinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of (5S)-5-[bis[3,5-bis(trifluoroMethyl)phenyl][[(1,1-diMethylethyl)diMethylsilyl]oxy]Methyl]-2-Pyrrolidinone

Chemical Property:

Purity/Quality:: >95%,>98%e.e. ^*data from raw suppliers

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Pictogram(s):
Hazard Codes:

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Technology Process of (5S)-5-[bis[3,5-bis(trifluoroMethyl)phenyl][[(1,1-diMethylethyl)diMethylsilyl]oxy]Methyl]-2-Pyrrolidinone

There total 1 articles about (5S)-5-[bis[3,5-bis(trifluoroMethyl)phenyl][[(1,1-diMethylethyl)diMethylsilyl]oxy]Methyl]-2-Pyrrolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1092807-24-3
(S)-5-{bis[3,5-bis(trifluoromethyl)phenyl](hydroxy)methyl}pyrrolidin-2-one

: 69739-34-0
t-butyldimethylsiyl triflate

: 1227364-30-8
C₂₇H₂₇F₁₂NO₂Si

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2010.02.122

Reference yield: 58.0%

: 1227364-30-8
C₂₇H₂₇F₁₂NO₂Si

: 122-51-0
orthoformic acid triethyl ester

: 100-63-0
phenylhydrazine

: BF₄^(1-)*C₃₄H₃₂F₁₂N₃OSi⁽¹⁺⁾

Guidance literature:: C₂₇H₂₇F₁₂NO₂Si; With trimethoxonium tetrafluoroborate; In dichloromethane; at 20 ℃; Inert atmosphere;

phenylhydrazine; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

orthoformic acid triethyl ester; In methanol; for 24h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2010.02.122