(Z)-3,7-Dimethyl-2,7-octadien-1-ol propanoate

Base Information

Chemical Name:(Z)-3,7-Dimethyl-2,7-octadien-1-ol propanoate
CAS No.:73214-62-7
Molecular Formula:C13H22O2
Molecular Weight:210.316
Hs Code.:
Mol file:73214-62-7.mol

Synonyms:(Z)-3,7-Dimethyl-2,7-octadien-1-ol propanoate;(Z)-3,7-Dimethyl-2,7-octadienyl propionate

Suppliers and Price of (Z)-3,7-Dimethyl-2,7-octadien-1-ol propanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of (Z)-3,7-Dimethyl-2,7-octadien-1-ol propanoate

Chemical Property:

PSA：26.30000
LogP:3.63230

Purity/Quality:: 99% ,98%,Electron Grade , ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-3,7-Dimethyl-2,7-octadien-1-ol propanoate

There total 3 articles about (Z)-3,7-Dimethyl-2,7-octadien-1-ol propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87081-71-8
(Z)-7-hydroxy-3,7-dimethyl-2-octen-1-yl propanoate

: 105-91-9,27751-90-2
(Z)-3,7-dimethyl-2,6-octadien-1-yl propanoate

: 73214-62-7
(Z)-3,7-dimethyl-2,7-octadien-1-yl propanoate

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane; at -5 ℃; for 0.666667h; Yield given. Yields of byproduct given;

Reference yield:

: 29021-98-5
3-(2-methyl-[1,3]dioxolan-2-yl)-propan-1-ol

: 73214-62-7
(Z)-3,7-dimethyl-2,7-octadien-1-yl propanoate

Guidance literature:: Multi-step reaction with 9 steps

1: 86 percent / pyridinium chlorochromate, sodium acetate / CH₂Cl₂ / 0.75 h / 25 °C

2: 1.) sodium hydride / 1.) ether, 25 deg C, 45 min, 2.) 3 h

3: 98 percent / hydrogen / 5percent Pd-C / methanol / 12 h / 25 °C

4: 93 percent / lithium aluminum hydride / diethyl ether / 2 h / 0 °C

5: 86 percent / hydrochloric acid / diethyl ether / 3 h / 25 °C

6: 97 percent / pyridine

7: 1.) sodium iodide, 2.) DBU / 1.) DMF, 50 deg C, 3.5 h, 2.) 80 deg C, 3.5 h

8: 1.) sodium hydride, 3.) aluminum chloride, lithium aluminum hydride / 1.) ether, 25 deg C, 1 h, 2.) 10 h, 3.) 0 deg C, 1 h

9: triethylamine / 24 h / 25 °C

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; hydrogen; sodium acetate; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; pyridinium chlorochromate; sodium iodide; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane;

Reference yield:

: 7-methyl-3-methylene-7-octenal diethyl acetal

: 79-03-8
propionyl chloride

: 73214-62-7
(Z)-3,7-dimethyl-2,7-octadien-1-yl propanoate

: 73214-63-8
7-methyl-3-methylene-7-octenyl propionate

: 75705-48-5
3,7-dimethyl-2(E),7-octadienyl-1-propionate

Guidance literature:: 7-methyl-3-methylene-7-octenal diethyl acetal; With formic acid; acetic acid; In water; at 70 - 80 ℃; for 8h;

With sodium tetrahydroborate; sodium hydroxide; In ethanol; water; at 15 - 20 ℃; for 16h; Inert atmosphere; Cooling with ice;

propionyl chloride; With pyridine; In tetrahydrofuran; for 19h; Inert atmosphere; Cooling with ice;