L-GLUCOSE

Base Information

• Chemical Name: L-GLUCOSE
• CAS No.: 393-92-0
• Molecular Formula: C6H12O6
• Molecular Weight: 180.16
• Mol file: 393-92-0.mol

Synonyms:GLUCOSE, L-;L-GLUCOPYRANOSE;L-(-)-GLUCOSE;L-GLUCOSE;Hexopyranose;L-GLUCOSE, 98%, MIXTURE OF ANOMERS;Cyazofamid, Pestanal;L-Glucose anhydrous, 98%

Chemical Property of L-GLUCOSE

Chemical Property:

• Melting Point: 153-156 °C(lit.)

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of L-GLUCOSE

There total 3 articles about L-GLUCOSE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

5-fluoro-2,4-dinitro-benzoic acid (393-93-1) → 5-fluoro-2,4-dinitrobenzoyl chloride (393-92-0)

Guidance literature:

With thionyl chloride; for 2.5h; Heating;

DOI:10.1002/jhet.5570240134

Reference yield:

m-Fluorotoluene (352-70-5) → 5-fluoro-2,4-dinitrobenzoyl chloride (393-92-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 81 percent / nitric acid (d=1.42), conc. sulphuric acid / 1.) not over 35 deg C; 2.) 30 min, room temp.

2: 53 percent / conc. sulphuric acid, anhydrous chromic acid / H₂O / 1.) 20 min, -6 deg C - 0 deg C; 2.) room temp., 3.5 h.

3: 75 percent / SOCl₂ / 2.5 h / Heating

With thionyl chloride; sulfuric acid; nitric acid; chromic acid; In water;

DOI:10.1002/jhet.5570240134

Reference yield:

1-fluoro-5-methyl-2,4-dinitro-benzene (349-01-9) → 5-fluoro-2,4-dinitrobenzoyl chloride (393-92-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 53 percent / conc. sulphuric acid, anhydrous chromic acid / H₂O / 1.) 20 min, -6 deg C - 0 deg C; 2.) room temp., 3.5 h.

2: 75 percent / SOCl₂ / 2.5 h / Heating

With thionyl chloride; sulfuric acid; chromic acid; In water;

DOI:10.1002/jhet.5570240134

upstream raw materials:

5-fluoro-2,4-dinitro-benzoic acid

m-Fluorotoluene

1-fluoro-5-methyl-2,4-dinitro-benzene

Downstream raw materials:

ethyl 3-cyclopropylamino-2-(5-fluoro-2,4-dinitrobenzoyl)acrylate

ethyl 3-cyclopropylamino-2-(5-hydroxy-2,4-dinitrobenzoyl)acrylate

ethyl 5-fluoro-2,4-dinitrobenzoylacetate

diethyl 5-fluoro-2,4-dinitrobenzoylmalonate