1-(2-Fluoro-4,5-dimethoxyphenyl)ethanone

Base Information

• Chemical Name: 1-(2-Fluoro-4,5-dimethoxyphenyl)ethanone
• CAS No.: 142265-69-8
• Molecular Formula: C₁₀H₁₁FO₃
• Molecular Weight: 198.19
• Hs Code.: 2914790090
• Mol file: 142265-69-8.mol

Synonyms:2'-fluoro-4',5'-dimethoxyacetophenone;1-(2-Fluoro-4,5-dimethoxyphenyl)ethanone;Ethanone, 1-(2-fluoro-4,5-dimethoxyphenyl)-;1-(2-Fluoro-4,5-dimethoxyphenyl)ethan-1-one

Chemical Property of 1-(2-Fluoro-4,5-dimethoxyphenyl)ethanone

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

99%+ ^*data from raw suppliers

1-(2-Fluoro-4,5-dimethoxyphenyl)ethanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(2-Fluoro-4,5-dimethoxyphenyl)ethanone

There total 2 articles about 1-(2-Fluoro-4,5-dimethoxyphenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.5%

4-fluoroveratrole (398-62-9) + acetyl chloride (75-36-5) → 1-(2-fluoro-4,5-dimethoxyphenyl)ethanone (142265-69-8)

Guidance literature:

With aluminium trichloride; In 1,2-dichloro-ethane; at -20 - 20 ℃; for 2.5h;

Reference yield:

1-(3,4-dimethoxyphenyl)ethanone (1131-62-0) → 1-(2-fluoro-4,5-dimethoxyphenyl)ethanone (142265-69-8)

Guidance literature:

With Selectfluor; at 70 ℃; for 20h; Ionic liquid;

DOI:10.3390/molecules14072394

Reference yield: 90.6%

1-(2-fluoro-4,5-dimethoxyphenyl)ethanone (142265-69-8) → 1-Ethyl-2-fluoro-4,5-dimethoxy-benzene (158641-46-4)

Guidance literature:

With hydrogen; acetic acid; palladium on activated charcoal; Ambient temperature;

upstream raw materials:

4-fluoroveratrole

acetyl chloride

1-(3,4-dimethoxyphenyl)ethanone

Downstream raw materials:

1-Ethyl-2-fluoro-4,5-dimethoxy-benzene

2-Bromo-1-(2-fluoro-4,5-dimethoxy-phenyl)-ethanone

4,5-dihydroxy-2-fluorobenzoic acid

2-fluoro-4,5-dimethoxybenzoic acid

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