diMethyl [1,1':4',1'':4'',1'''-quaterphenyl]-2'',3'-dicarboxylate

Base Information

Chemical Name:diMethyl [1,1':4',1'':4'',1'''-quaterphenyl]-2'',3'-dicarboxylate
CAS No.:119598-33-3
Molecular Formula:C28H22O4
Molecular Weight:422.48
Hs Code.:
Mol file:119598-33-3.mol

Synonyms:diMethyl [1,1':4',1'':4'',1'''-quaterphenyl]-2'',3'-dicarboxylate

Suppliers and Price of diMethyl [1,1':4',1'':4'',1'''-quaterphenyl]-2'',3'-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of diMethyl [1,1':4',1'':4'',1'''-quaterphenyl]-2'',3'-dicarboxylate

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of diMethyl [1,1':4',1'':4'',1'''-quaterphenyl]-2'',3'-dicarboxylate

There total 2 articles about diMethyl [1,1':4',1'':4'',1'''-quaterphenyl]-2'',3'-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 716-76-7
3-phenylbenzoic acid

: 74-88-4
methyl iodide

: 119598-33-3
p-Quaterphenyl-dicarbonsaeure-(2'.3')-dimethylester

Guidance literature:: 3-phenylbenzoic acid; With rhodium(III) chloride trihydrate; tetrabutylammonium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 20h; Electrolysis;

methyl iodide;
DOI:10.1021/acscatal.1c01127

Reference yield:

: 67-56-1
methanol

: 124143-35-7
[1,1';4',1'';4'',1''']quaterphenyl-3',2''-dicarboxylic acid

: 119598-33-3
p-Quaterphenyl-dicarbonsaeure-(2'.3')-dimethylester

Guidance literature:: With hydrogenchloride;
DOI:10.1021/jo01066a012

Reference yield:

: 119598-33-3
p-Quaterphenyl-dicarbonsaeure-(2'.3')-dimethylester

: 37634-87-0
2,7-Diphenylphenanthrene

Guidance literature:: Multi-step reaction with 4 steps

1: LiAlH₄

2: PBr₃, Py / benzene

3: PhLi

4: Pd-C

With pyridine; lithium aluminium tetrahydride; phosphorus tribromide; phenyllithium; palladium on activated charcoal; In benzene;
DOI:10.1021/jo01066a012