N,N-Dibenzylbenzamide

Base Information

• Chemical Name: N,N-Dibenzylbenzamide
• CAS No.: 23825-35-6
• Molecular Formula: C21H19 N O
• Molecular Weight: 301.388
• European Community (EC) Number: 653-603-1
• NSC Number: 406284
• DSSTox Substance ID: DTXSID00178531
• Nikkaji Number: J867.887A
• Wikidata: Q83048963
• ChEMBL ID: CHEMBL1453901
• Mol file: 23825-35-6.mol

Synonyms:N,N-Dibenzylbenzamide;Benzamide, N,N-dibenzyl-;Benzamide, N,N-bis(phenylmethyl)-;23825-35-6;BRN 2218227;AI3-01075;Oprea1_018240;MLS001185448;N~1~,N~1~-dibenzylbenzamide;SCHEMBL1003508;CHEMBL1453901;DTXSID00178531;HMS2836G24;ADAL1038702;NSC406284;STK078318;AKOS002707448;NSC 406284;NSC-406284;NCGC00247314-01;LS-26307;SMR000502147;AE-848/00895029

Chemical Property of N,N-Dibenzylbenzamide

Chemical Property:

• Boiling Point: 493.2°Cat760mmHg
• Flash Point: 232.1°C
• Density: 1.132g/cm³
• XLogP3: 4.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 5
• Exact Mass: 301.146664230
• Heavy Atom Count: 23
• Complexity: 329

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CN(CC2=CC=CC=C2)C(=O)C3=CC=CC=C3

Technology Process of N,N-Dibenzylbenzamide

There total 62 articles about N,N-Dibenzylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

benzoic acid (65-85-0,8013-63-6) + dibenzylamine (103-49-1) → N,N-dibenzylbenzamide (23825-35-6)

Guidance literature:

With S=P(Cl)(2-oxazolone-3-yl)2; triethylamine; In acetonitrile; for 1.5h; Ambient temperature;

Reference yield: 99.0%

benzoyl chloride (98-88-4) + dibenzylamine (103-49-1) → N,N-dibenzylbenzamide (23825-35-6)

Guidance literature:

benzoyl chloride; dibenzylamine; With triethylamine; In dichloromethane; at 20 ℃; for 0.333333h;

With poly{trans-bicyclo[2.2.1]hept-5-ene-2,3-di(chlorocarbonyl)}; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1021/ol0352759

Reference yield: 95.0%

iodobenzene (591-50-4) + carbon monoxide (201230-82-2) + dibenzylamine (103-49-1) → N,N-dibenzylbenzamide (23825-35-6)

Guidance literature:

With triethylamine; In toluene; at 100 ℃; for 8h; under 3750.38 Torr; Inert atmosphere;

DOI:10.1039/c5ra18692g

upstream raw materials:

tribenzylamine

2-Benzoyloxy-1-(p-toluol-sulfonyl)-propen-⁽²⁾

dibenzylamine

PhC(O)N(CH₂Cl)2

Downstream raw materials:

(S)-3-(4-nitrophenyl)isobenzofuran-1(3H)-one

tribenzylamine hydrochloride

tribenzylamine

dibenzylamine