4-Cyano-2-nitrophenethyl acetate

Base Information

Chemical Name:4-Cyano-2-nitrophenethyl acetate
CAS No.:134403-89-7
Molecular Formula:C11H10N2O4
Molecular Weight:234.2081
Hs Code.:2926909090
Mol file:134403-89-7.mol

Synonyms:4-Cyano-2-nitrophenethyl acetate

Suppliers and Price of 4-Cyano-2-nitrophenethyl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4-Cyano-2-nitrophenethylacetate 95+%
1g
$ 608.00

Alichem
4-Cyano-2-nitrophenethylacetate
1g
$ 534.60

Total 2 raw suppliers

Chemical Property of 4-Cyano-2-nitrophenethyl acetate

Chemical Property:

PSA：95.91000
LogP:2.09528

Purity/Quality:

≥99% ^*data from raw suppliers

4-Cyano-2-nitrophenethylacetate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Cyano-2-nitrophenethyl acetate

There total 5 articles about 4-Cyano-2-nitrophenethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69395-13-7
4-(2-hydroxyethyl)benzonitrile

: 134403-89-7
4-(2-acetyloxyethyl)-3-nitrobenzonitrile

Guidance literature:: nitration;
DOI:10.1016/0040-4039(91)80371-C

Reference yield:

: 100-27-6
2-(4-nitrophenyl)ethanol

: 134403-89-7
4-(2-acetyloxyethyl)-3-nitrobenzonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 16.2 g / H₂ / PtO₂ / aq. ethanol

2: 1.) HCl, NaNO₂; 2.) Cu₂Cl₂ / H₂O / 1.) 3 deg C; 2.) 3-50 deg C, 4 h

3: acetic anhydride / 0.5 h / Ambient temperature

4: H₂SO₄, HNO₃ / 2.5 h / 0 - 5 °C

With copper(I) chloride; hydrogenchloride; sulfuric acid; hydrogen; nitric acid; sodium nitrite; platinum(IV) oxide; In ethanol; water; acetic anhydride;
DOI:10.1002/hlca.19810640547

Reference yield:

: 103-45-7
acetic acid phenethyl ester

: 134403-89-7
4-(2-acetyloxyethyl)-3-nitrobenzonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) H₂SO₄, HNO₃; 2.) HCl / 1.) acetic anhydride, -15 deg C, 105 min; 2.) methanol, reflux, 3.5 h

2: 16.2 g / H₂ / PtO₂ / aq. ethanol

3: 1.) HCl, NaNO₂; 2.) Cu₂Cl₂ / H₂O / 1.) 3 deg C; 2.) 3-50 deg C, 4 h

4: acetic anhydride / 0.5 h / Ambient temperature

5: H₂SO₄, HNO₃ / 2.5 h / 0 - 5 °C

With copper(I) chloride; hydrogenchloride; sulfuric acid; hydrogen; nitric acid; sodium nitrite; platinum(IV) oxide; In ethanol; water; acetic anhydride;
DOI:10.1002/hlca.19810640547